Plasma-assisted elaboration of macropore architectures in titanium nitride

被引：4

作者：

Wang, Qiushi ^{[1
]}

Li, Yingai ^{[1
]}

Zhang, Jian ^{[1
]}

Jin, Yunxia ^{[1
]}

Huang, Dahai ^{[1
]}

Wu, Si ^{[1
]}

Cu, Qiliang ^{[1
]}

Zou, Guangtian ^{[1
]}

机构：

[1] Jilin Univ, State Key Lab Superhard Mat, Changchun 130012, Peoples R China

来源：

JOURNAL OF ALLOYS AND COMPOUNDS | 2010年 / 494卷 / 1-2期

基金：

高等学校博士学科点专项科研基金;

关键词：

Titanium nitride; Macroporous material; Gas absorbing material; Plasma-assisted growth; CHEMICAL-VAPOR-DEPOSITION; SURFACE-AREA; TIN; FILMS; COATINGS; NITROGEN; POROSITY; ROUTE; OXIDE; TIO2;

D O I：

10.1016/j.jallcom.2010.01.067

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Titanium nitride (TiN) is prepared via a convenient direct nitridation process in an improved direct current arc discharge plasma setup. The XRD pattern shows that the as-prepared coarse particles are single-phase TIN possessing a face-centered cubic lattice with the cell constant a = 0.4242 nm. SEM studies reveal that the TiN powders are composed of unique macropore architectures with the pore sizes in the range of 0.2-2.0 mu M and the thickness of the side walls in the range of 0.2-0.5 mu M. The macroporous nature of the obtained TiN sample is further confirmed by N-2 adsorption-desorption measurements, through which a specific surface area to be about 13.57 m(2) g(-1) is determined by using the BET gas adsorption method. (C) 2010 Elsevier B.V. All rights reserved.

引用

页码：L11 / L14

页数：4

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