Structural and magnetic properties of nickel-zinc ferrite nanocrystalline magnetic particles prepared by microwave combustion method

被引：10
|
作者：
Parmar, H. [1 ]
Upadhyay, R. V. [1 ]
Rayaprol, S. [2 ]
Siruguri, V. [2 ]
机构：
[1] Charotar Univ Sci & Technol, PD Patel Inst Appl Sci, Changa 388421, Gujarat, India
[2] Bhabha Atom Res Ctr, Mumbai Ctr, UGC DAE Consortium Sci Res, Mumbai 400085, Maharashtra, India
来源：
INDIAN JOURNAL OF PHYSICS | 2014年 / 88卷 / 12期
关键词：
Neutron diffraction; Magnetic nano-crystalline; Microwave induced Combustion method; ZN FERRITES; NANOPARTICLES; TEMPERATURE;
D O I：
10.1007/s12648-014-0576-5
中图分类号：
O4 [物理学];
学科分类号：
0702 ;
摘要：
Magnetic, nano-crystalline samples of zinc substituted nickel ferrite, (ZnxNi1-xFe2O4 for x = 0.0-0.9 in step of 0.2), are synthesized using microwave combustion synthesis technique. The structural properties of Ni-Zn are determined using X-ray powder diffraction, transmission electron microscopy; Fourier transforms infrared spectroscopy and neutron diffraction techniques. Average crystalline size obtained from X-ray diffraction and neutron diffraction is in the range of 30-60 nm. The cation distribution obtained from X-ray diffraction and neutron diffraction show that Zn occupies only tetrahedral A-site in the spinel lattice. The values of magnetic moment derived from magnetization measurements and neutron diffraction agrees nearly 97 % to that of bulk at 300 K. This methodology can be used to prepare large quantities (about 10 g) of sample at one time using kitchen microwave oven working at 1,200 W power.
引用
收藏
页码：1257 / 1264
页数：8
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