Synthesis and characterization of binuclear rhenium(I) complexes containing bifunctional ligands

被引：5

作者：

Klausmeyer, Kevin K. ^{[1
]}

Beckles, Franklin R. ^{[1
]}

机构：

[1] Baylor Univ, Dept Chem & Biochem, Waco, TX 76798 USA

来源：

INORGANICA CHIMICA ACTA | 2007年 / 360卷 / 10期

基金：

美国国家科学基金会;

关键词：

rhenium carbonyl; carboxylate compounds; ligand exchange; bifunctional ligands;

D O I：

10.1016/j.ica.2007.03.034

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The ligand exchange reaction of the anionic binuclear rhenium complexes Re-2 (CO)(6) (OR)(3)(-) (R = H (1), or Me (2)) has been studied with the bifunctional ligands 2-aminophenol (3), 4-hydroxypyridine (4), 3-hydroxybenzoic acid (5), and 3-pyridylcarbinol (6). The reactivity the pendant pyridyl group of 6 was studied in reactions with the Lewis acids ZnCl2 (7), and AgPF6 (8). Crystal structure determinations for several of these derivatives have been carried out which reveal both discrete and polymeric complexes upon addition of the Lewis base. (c) 2007 Elsevier B.V. All rights reserved.

引用

页码：3241 / 3249

页数：9

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