Dielectric spectroscopy and structural characterization of nano-filler-loaded epoxy resin

被引：26
|
作者：
Thakor, S. G. [1 ]
Rana, V. A. [1 ]
Vankar, H. P. [1 ]
Pandit, T. R. [1 ]
机构：
[1] Gujarat Univ, Sch Sci, Dept Phys, Ahmadabad 380009, Gujarat, India
来源：
JOURNAL OF ADVANCED DIELECTRICS | 2021年 / 11卷 / 02期
关键词：
Epoxy resin; nano-fillers; dielectric relaxation spectroscopy; FTIR; mechanical properties; XRD; IMPROVED THERMAL-CONDUCTIVITY; MECHANICAL-PROPERTIES; FREQUENCY-RANGE; ALPHA-AL2O3; NANOPARTICLES; ELECTRICAL-PROPERTIES; TIO2; ZNO NANOPARTICLES; WATER-ABSORPTION; BORON-NITRIDE; MHZ;
D O I：
10.1142/S2010135X21500119
中图分类号：
O59 [应用物理学];
学科分类号：
摘要：
This work outlines the characterization of epoxy resin [Bisphenol A-(epichlorhydrin): epoxy] and hardener [N(3-dimethylaminopropyl)-1,3-propylenediamine] with various inorganic nano-fillers. Dielectric characterizations of epoxy, hardener, neat epoxy (epoxy + hardener) and nano-epoxy (nano-filler + neat epoxy) composites loaded with 1 wt.% of inorganic nano-fillers (SiO2, Al2O3, TiO2 and ZnO) were carried out using precision LCR meter, over the frequency range of 1 kHz-2 MHz at a constant temperature of 300.15 K. The structural information of nano-fillers, neat epoxy and nano-epoxy composites was understood by Fourier transform infrared spectroscopy and by XRD. Moreover, hardness and shear strength (shear punch) were also determined in order to gain additional information about the mechanical properties of epoxy composite. Influence of inorganic nano-fillers on the dielectric properties, structural chemistry and mechanical properties of neat epoxy composite is discussed thoroughly in this study.
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页数：12
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