PHOSPHORYLATED THIACALIX[6]ARENE: SYNTHESIS AND CHARACTERIZATION OF HOST-GUEST COMPLEX OF SELECTIVE Pd2+ ION EXTRACTION

被引：5
|
作者：
Ulzii, Munkhtuya [1 ]
Rao, Kunda Uma Maheswara [2 ]
Yamada, Manabu [3 ]
Hamada, Fumio [1 ]
机构：
[1] Akita Univ, Grad Sch Engn & Resource Sci, Dept Appl Chem Environm, Akita 0108502, Japan
[2] Akita Univ, Venture Business Lab, Akita 0108502, Japan
[3] Akita Univ, Grad Sch Engn & Resource Sci, Res Ctr Engn Sci, Akita 0108502, Japan
来源：
HETEROCYCLES | 2014年 / 89卷 / 11期
关键词：
Phosphorylated Thiacalix[6]arene; Pd2+ Ion Extraction; AUTOMOTIVE CATALYST RESIDUE; THIACALIXARENES; CALIXARENES; RECOGNITION; RECOVERY; AU(III); PD(II); ACID;
D O I：
10.3987/COM-14-13083
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
New phosphorylated thiacalix[6]arene was synthesized and its metal extraction ability was examined by using automotive catalyst residue solution. The new host molecule showed high affinity towards Pd2+ ion and reasonable affinity towards other metals. Then we studied the effect of concentration and time on the Pd2+ ion extraction using Pd2+ ion standard solution. In addition to this, we successfully characterized the host-guest complex formed during Pd2+ ion extraction by using Job's method, P-31 & H-1 NMR, IR and elemental analysis.
引用
收藏
页码：2554 / 2561
页数：8
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