Synthesis and crystal structure of one dimensional chain manganese complex [Mn2(C7H4O3)4(CH3OH)2]•4H2O•2CH3OH

被引：0
|
作者：
Li, JA [1 ]
Zhang, FX
Wu, AZ
Shi, QZ
Li, YZ
Wang, LF
机构：
[1] NW Univ Xian, Shanxi Key Lab Phosicoinorgan Chem, Xian 710069, Peoples R China
[2] Lanzhou Univ, Dept Chem, Lanzhou 730000, Peoples R China
来源：
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY | 2003年 / 22卷 / 01期
关键词：
one dimensional chain manganese (IV) complex; crystal structure; synthesis;
D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The one dimensional chain manganese complex [Mn-2(C7H4O3)(4)(CH3OH)(2)].4H(2)O.2CH(3)OH has been synthesized, and it was characterized by IR, X-ray diffraction and UV-Vis. X-ray diffraction result shows that the crystal belongs to triclinic, space group P (1) over bar with a = 7.653(5), b = 10.486(7), c = 12.943(8) Angstrom, alpha = 103.24(1), beta = 104.55(1), gamma = 110.11(1)degrees, V = 885.4(9) Angstrom(3) and Z = 1. UV-Vis spectrum result indicates there exists a peak at 547 nm, corresponding to the electron transition of d-d.
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页码：93 / 96
页数：4
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