Simultaneous Analysis of Selected Typical Antibiotics in Manure by Microwave-Assisted Extraction and LC-MS n

被引：38
|
作者：
Hu, Xiangang [1 ]
Luo, Yi [1 ]
Zhou, Qixing [1 ,2 ]
机构：
[1] Nankai Univ, Key Lab Pollut Proc & Environm Criteria, Minist Educ, Coll Environm Sci & Engn, Tianjin 300071, Peoples R China
[2] Chinese Acad Sci, Inst Appl Ecol, Key Lab Terr Ecol Proc, Shenyang 110016, Peoples R China
来源：
CHROMATOGRAPHIA | 2010年 / 71卷 / 3-4期
基金：
美国国家科学基金会;
关键词：
Column liquid chromatography; Microwave-assisted extraction; Mass spectrometry; Tetracyclines; Sulfonamides; Fluoroquinolones; Manure; CAPILLARY-ZONE-ELECTROPHORESIS; LIQUID-CHROMATOGRAPHY; WASTE-WATER; VETERINARY ANTIBIOTICS; ANIMAL MANURE; TETRACYCLINE; SULFONAMIDES; SOILS; TRIMETHOPRIM; RESIDUES;
D O I：
10.1365/s10337-009-1438-8
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
Analysis of antibiotics in the environment has become an urgent issue. A novel method entailing microwave-assisted extraction (MAE) and high-performance liquid chromatography-electrospray mass spectrometry (LC-MS (n) ) has been developed for determination of selected typical antibiotics, including quinolones, sulfonamides, and tetracyclines, in manure. Compared with ultrasonic extraction, MAE significantly increased recovery of fluoroquinolones (63-106%), sulfonamides (64-133%), and tetracyclines (64-109%) from manure. Acetonitrile acidified with formic acid buffer solution (pH 4.0) was used for extraction of swine manure whereas chicken manure was extracted with 0.1 M EDTA-McIlvaine buffer solution. Limits of quantification (LOQ) for all compounds were in the range 5.12-168.4 mu g kg(-1) dry matter, which were satisfactory for analysis of all samples. The suitability of the method was assessed by analysis of manure from six different sites.
引用
收藏
页码：217 / 223
页数：7
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