Synthesis and Characterization of Azacyclophanes Containing 1,3,5-Triazine

被引:0
|
作者
Lue, Guohua [1 ]
Hua, Chengwen [1 ]
Gou, Xiaofeng [1 ]
Liu, Yanfeng [1 ]
机构
[1] NW Univ Xian, Coll Chem & Mat Sci, Minist Educ, Key Lab Synthet & Nat Funct Mol Chem, Xian 710069, Peoples R China
关键词
cyanuric chloride; cyclophane; synthesis; characterization; MACROCYCLIC LIGANDS;
D O I
暂无
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
Cyclophane with a cavity structure, has a great potential prospects. Some novel azacyclophanes were synthesized from cyanuric chloride, phenol, sodium methoxide, 1,6-hexane diamine and 4,4'-diamino-diphenyl methane by substitution, and their structures were characterized by H-1 NMR, IR, MALDI-TOF-MS techniques and elemental analysis. A large number of experiments have been carried out to explore the solvent, alkal and concentration to find out the best reaction conditions.
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页码:745 / 748
页数:4
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