Alaptide from synchrotron powder diffraction data

被引:2
|
作者
Rohlicek, Jan [1 ]
Maixner, Jaroslav [2 ]
Pazout, Richard [2 ]
Husak, Michal [1 ]
Cibulkova, Jana [2 ]
Kratochvil, Bohumil [1 ]
机构
[1] Prague Inst Chem Technol, Dept Solid State Chem, CR-16628 Prague 6, Czech Republic
[2] Prague Inst Chem Technol, Cent Labs, CR-16628 Prague 6, Czech Republic
关键词
D O I
10.1107/S1600536810007750
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound [systematic name: (8S)-8-methyl-6,9-diazaspiro[ 4.5]decane-7,10-dione], C9H14N2O2, consists of two connected rings, viz. a piperazine-2,5-dione (DKP) ring and a five-membered ring. The DKP ring adopts a slight boat conformation and the bonded methyl group is in an equatorial position. The five-membered ring is in an envelope conformation. In the crystal structure, intermolecular N-H center dot center dot center dot O hydrogen bonds link molecules into chains running parallel to the c axis.
引用
收藏
页码:O821 / U2229
页数:10
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