Synthesis and characterization of cu nanoparticles prepared by thermal decomposition of Cu-oleate complex

被引：2

作者：

Kang, Young Soo ^{[1
]}

Kim, Young Wan ^{[1
]}

Jo, Beong Gi ^{[1
]}

Jeong, Jee Hean ^{[1
]}

机构：

[1] Pukyong Natl Univ, Dept Chem, 599-1,Daeyeondong, Pusan 608737, South Korea

来源：

INTERNATIONAL JOURNAL OF NANOSCIENCE, VOL 5, NOS 2 AND 3 | 2006年 / 5卷 / 2-3期

关键词：

Cu nanoparticle; thermal decomposition; oleate capping;

D O I：

10.1142/S0219581X06004449

中图分类号：

TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

Cu nanoparticles have been synthesized by thermal decomposition of Cu-oleate complex, which was prepared by the reaction with CuCl2 and sodium oleate in water solution. The monodispersed Cu nanoparticles were produced by controlling temperature (290 degrees C). TEM images of the nanoparticles showed two-dimensional assembly of particles with diameter of 16.2 +/- 2.9 run, demonstrating the uniformity of these nanoparticles. EDX spectrum and XRD peaks of the nanoparticles showed the highly crystalline nature of the Cu structures. The decomposition of Cu-oleate complex was analyzed with TGA and the crystallization of Cu nanoparticles was observed with XRD.

引用

页码：339 / +

页数：2

共 50 条

[1] Synthesis and characterization of Cu nanoparticles prepared by thermal decomposition of Cu-oleate complex
Department of Chemistry, Pukyong National University, 599-1, Daeyeondong, Namgu Busan, 608-737, Korea, Republic of
不详
Int. J. Nanosci., 2006, 2-3 (339-344):
[2] Synthesis of cu nanoparticles prepared by using thermal decomposition of Cu-oleate complex
Kim, YH
Kang, YS
Lee, WJ
Jo, BG
Jeong, JH
MOLECULAR CRYSTALS AND LIQUID CRYSTALS, 2006, 445 (231/[521]-238/[528]) : 231 - 238
[3] Synthesis of oleate capped Cu nanoparticles by thermal decomposition
Kim, Young Hwan
Lee, Don Keun
Jo, Beong Gi
Jeong, Ji Hean
Kang, Young Soo
COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS, 2006, 284 : 364 - 368
[4] Modeling the Kinetics of Heavy Crude Oil Cu-Oleate Aquathermolysis
Tirado, Alexis
Felix, Guillermo
Suwaid, Muneer A.
Al-Muntaser, Ameen A.
Antonenko, Dmitry A.
Afanasiev, Igor S.
Varfolomeev, Mikhail A.
Yuan, Chengdong
Ancheyta, Jorge
INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH, 2023, 62 (23) : 9114 - 9122
[5] Solvent-free synthesis of monodisperse Cu nanoparticles by thermal decomposition of an oleylamine-coordinated Cu oxalate complex
Togashi, Takanari
Nakayama, Masato
Hashimoto, Atsuki
Ishizaki, Manabu
Kanaizuka, Katsuhiko
Kurihara, Masato
DALTON TRANSACTIONS, 2018, 47 (15) : 5342 - 5347
[6] The thermal behavior of the synthesis of Cu-BTA composite nanoparticles by thermal decomposition
Kao, Mu-Jung
Hsu, Fu-Chun
Guo, Jia-Bin
CURRENT APPLIED PHYSICS, 2013, 13 : S79 - S83
[7] Synthesis, Characterization and Catalytic Activity of Cu/Cu2O Nanoparticles Prepared in Aqueous Medium
Badawy, Sayed M.
El-Khashab, R. A.
Nayl, A. A.
BULLETIN OF CHEMICAL REACTION ENGINEERING AND CATALYSIS, 2015, 10 (02): : 169 - 174
[8] Size and Shape Controllable Synthesis of Monodisperse Iron Oxide Nanoparticles by Thermal Decomposition of Iron Oleate Complex
Chen, Zhongping
SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY, 2012, 42 (07) : 1040 - 1046
[9] Synthesis and characterization of ZnO nanoparticles by thermal decomposition of a curcumin zinc complex
Khalil, Mutasim I.
Al-Qunaibit, Maha M.
Al-Zahem, Aisha M.
Labis, Joselito P.
ARABIAN JOURNAL OF CHEMISTRY, 2014, 7 (06) : 1178 - 1184
[10] Synthesis of Cu Nanoparticles: Stability and Conversion into Cu2S Nanoparticles by Decomposition of Alkanethiolate
Rohner, Christian
Pekkari, Anna
Harelind, Hanna
Moth-Poulsend, Kasper
LANGMUIR, 2017, 33 (46) : 13272 - 13276

← 1 2 3 4 5 →