Raman spectroscopy for the investigation of indentation-induced domain texturing in lead zirconate titanate piezoceramics

被引:16
|
作者
Deluca, Marco [1 ,2 ]
Bermejo, Raul [1 ]
Gruenbichler, Hannes [1 ,2 ]
Presser, Volker [3 ]
Danzer, Robert [1 ,2 ]
Nickel, Klaus G. [4 ]
机构
[1] Univ Leoben, Inst Strukt & Funkt Keram, A-8700 Leoben, Austria
[2] Mat Ctr Leoben Forsch GmbH, A-8700 Leoben, Austria
[3] Drexel Univ, AJ Drexel Nanotechnol Inst, Philadelphia, PA 19104 USA
[4] Univ Tubingen, Inst Geosci, D-72074 Tubingen, Germany
关键词
Perovskites; PZT; Raman spectroscopy; Micro-indentation; FRACTURE-TOUGHNESS; ELECTRIC-FIELD; R-CURVE; CERAMICS; BEHAVIOR; ORIENTATION;
D O I
10.1016/j.scriptamat.2010.04.040
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The study of the close relationship between crack propagation and domain switching is of extreme importance in the reliability of PbZr1-xTixO3 (PZT) devices. We performed domain imaging in the neighbourhood of indentation cracks on poled and non-poled PZT bulk specimens using polarized micro-Raman spectroscopy. Non-destructive Raman measurements helped to correlate the indentation-induced domain texture with the crack growth resistance on both samples. Hence, polarized micro-Raman spectroscopy offers the potential to locally investigate regions of interest in complex piezoelectric devices. (C) 2010 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
引用
收藏
页码:343 / 346
页数:4
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