Nanosized silver(I) coordination networks of mixed bix-diphosphine (bix=1,4-bis(imidazol-1-ylmethyl)benzene)

被引：75
|
作者：
Zhang, L [1 ]
Lü, XQ [1 ]
Chen, CL [1 ]
Tan, HY [1 ]
Zhang, HX [1 ]
Kang, BS [1 ]
机构：
[1] Sun Yat Sen Univ, Sch Chem & Chem Engn, Guangzhou 510275, Peoples R China
来源：
CRYSTAL GROWTH & DESIGN | 2005年 / 5卷 / 01期
关键词：
D O I：
10.1021/cg049883m
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Assembly of silver(l) salts and bix in the presence of diphosphines provided four polymeric complexes [Ag(bix)(dppe)](n)(.)nBF(4) (1), [Ag(bix)(dppp)](n)(.)nPF(6) (2), [Ag(bix)(dppe)](n)-nPF(6)-nCH(3)OH (3), and [Ag(bix)(dppe)](n)(.)nSbF(6)(.) nCH(3)OH (4). X-ray diffraction analyses reveal that both 1 and 2 have a two-dimensional network composed of nanosized metallocyles, and the [Ag(bix)],, chains in 2 show alternate left and right helices. Complexes 3 and 4 are isomorphous, and they have 3D open frameworks of diamondoid topology with the size of 13 x 13 Angstrom(2) along the b-axis. Possible formation processes were interpreted by ESI-MS results.
引用
收藏
页码：283 / 287
页数：5
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