An easy conversion of the Baylis-Hillman adducts into tert-butyldimethylsilyl ethers with tert-butyldimethylsilyl chloride and Li2S

被引：4
|
作者：
Mamaghani, M [1 ]
Badrian, A [1 ]
机构：
[1] Guilan Univ, Fac Sci, Dept Chem, Rasht, Iran
来源：
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2004年 / 179卷 / 12期
关键词：
Baylis-Hillman adducts; tert-butyldimethylsilyl ethers; TBDMSCI; protecting group;
D O I：
10.1080/10426500490485291
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The hydroxy group of the Baylis-Hillman adducts is protected with the t-butyldimethylsilyl (TBDMS) group using the reaction of adducts 1a-h with tert-butyldimethylsilyl chloride (TBDMSCl) in the presence of lithium sulfide under nearly acidic reaction conditions.
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页码：2429 / 2435
页数：7
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