Solid state reactions in the Fe-Sn system under mechanical alloying and grinding

被引:20
|
作者
Yelsukov, EP
Dorofeev, GA
Barinov, VA
Grigor'eva, TF
Boldyrev, VV
机构
[1] RAS, Phys Tech Inst, Izhevsk 426001, Russia
[2] RAS, Inst Met Phys, Ekaterinburg 620219, Russia
[3] RAS, Inst Solid State Chem, Novosibirsk 630128, Russia
关键词
mechanical alloying and grinding; supersaturated nanocrystalline; solid solution; Mossbauer spectroscopy; X-ray diffraction;
D O I
10.4028/www.scientific.net/MSF.269-272.151
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Structure-phase transformations in the 68Fe-32Sn system by mechanical alloying from pure elements and mechanical grinding of a multi-phase alloy for different conditions of mechanical treatment in planetary ball mills were studied by X-ray diffraction, Fe-57 Mossbauer spectroscopy and magnetic measurements. The initial stages of structure-phase transformations by mechanical alloying and grinding were found to be different. However, the final product in all cases was nanocrystalline supersaturated solid solution of Sn in alpha-Fe with the bcc lattice parameter a= 0.2995 nm, the magnetic moment per Fe atom mu(Fe)=1.9 mu(B) and the Curie temperature T-c=700 K.
引用
收藏
页码:151 / 156
页数:6
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