High-resolution mass spectra of biotinylated, HEG-spacered molecular probes with oligosaccharide fragments of the capsular polysaccharides from Streptococcus pneumoniae

被引：7

作者：

Chizhov, Alexander O. ^{[1
]}

Sukhova, Elena V. ^{[1
]}

Khatuntseva, Elena A. ^{[1
]}

Tsvetkov, Yury E. ^{[1
]}

Nifantiev, Nikolay E. ^{[1
]}

机构：

[1] Russian Acad Sci, ND Zelinsky Inst Organ Chem, Moscow 119991, Russia

来源：

MENDELEEV COMMUNICATIONS | 2015年 / 25卷 / 06期

基金：

俄罗斯科学基金会;

关键词：

SPECTROMETRY; TRISACCHARIDE; REAGENTS; SYSTEM;

D O I：

10.1016/j.mencom.2015.11.020

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

High-resolution electrospray mass spectra (MS and MS/MS) of biotinylated, hexaethylene glycol (HEG) spacered molecular probes bearing immunogenic oligosaccharides, fragments of capsular polysaccharides of Streptococcus pneumoniae, were interpreted (four examples). Characteristic fragmentation of the aglycone at the end of the HEG chain distant from the biotin fragment has been revealed.

引用

页码：457 / 459

页数：3

共 6 条

[1] Gas-Phase Fragmentation Studies of Biotinylated, Hexaethylene Glycol–Spacered Oligosaccharides—Molecular Probes—Using Electrospray Mass Spectrometry on a Hybrid High-Resolution Mass Spectrometer
Chizhov, A.O. (chizhov@ioc.ac.ru), 1600, Maik Nauka Publishing / Springer SBM (72):
[2] Gas-Phase Fragmentation Studies of Biotinylated, Hexaethylene Glycol–Spacered Oligosaccharides—Molecular Probes—Using Electrospray Mass Spectrometry on a Hybrid High-Resolution Mass Spectrometer
A. O. Chizhov
D. A. Argunov
M. L. Gening
E. V. Sukhova
E. A. Khatuntseva
A. A. Karelin
B. S. Komarova
M. V. Orekhova
V. B. Krylov
D. V. Yasunskii
Yu. E. Tsvetkov
N. E. Nifantiev
Journal of Analytical Chemistry, 2017, 72 : 1312 - 1321
[3] Gas-Phase Fragmentation Studies of Biotinylated, Hexaethylene Glycol-Spacered Oligosaccharides-Molecular Probes-Using Electrospray Mass Spectrometry on a Hybrid High-Resolution Mass Spectrometer
Chizhov, A. O.
Argunov, D. A.
Gening, M. L.
Sukhova, E. V.
Khatuntseva, E. A.
Karelin, A. A.
Komarova, B. S.
Orekhova, M. V.
Krylov, V. B.
Yasunskii, D. V.
Tsvetkov, Yu. E.
Nifantiev, N. E.
JOURNAL OF ANALYTICAL CHEMISTRY, 2017, 72 (13) : 1312 - 1321
[4] The use of biotinylated oligosaccharides related to fragments of capsular polysaccharides from Streptococcus pneumoniae serotypes 3 and 14 as a tool for assessment of the level of vaccine-induced antibody response to neoglycoconjugates
E. A. Kurbatova
E. A. Akhmatova
N. K. Akhmatova
N. B. Egorova
N. E. Yastrebova
E. E. Romanenko
A. Yu. Leonova
A. V. Poddubikov
Yu. E. Tsvetkov
E. V. Sukhova
M. L. Gening
D. V. Yashunsky
N. E. Nifantiev
Russian Chemical Bulletin, 2016, 65 : 1608 - 1616
[5] The use of biotinylated oligosaccharides related to fragments of capsular polysaccharides from Streptococcus pneumoniae serotypes 3 and 14 as a tool for assessment of the level of vaccine-induced antibody response to neoglycoconjugates
Kurbatova, E. A.
Akhmatova, E. A.
Akhmatova, N. K.
Egorova, N. B.
Yastrebova, N. E.
Romanenko, E. E.
Leonova, A. Yu.
Poddubikov, A. V.
Tsvetkov, Yu. E.
Sukhova, E. V.
Gening, M. L.
Yashunsky, D. V.
Nifantiev, N. E.
RUSSIAN CHEMICAL BULLETIN, 2016, 65 (06) : 1608 - 1616
[6] High-resolution electrospray mass spectra of hexaethylene glycol connected biotinylated HNK-1 antigenic trisaccharide molecular probe and its non-sulfated analogue
Chizhov, Alexander O.
Sukhova, Elena V.
Khatuntseva, Elena A.
Tsvetkov, Yury E.
Gening, Marina L.
Nifantiev, Nikolay E.
CARBOHYDRATE RESEARCH, 2015, 417 : 15 - 18

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