Influence of proton chemical-shift anisotropy on magic-angle spinning spectra of hydrate crystals

被引:13
|
作者
Tekely, P
Palmas, P
Mutzenhardt, P
机构
[1] Lab. de Méthodologie RMN, UA CNRS 406, Université H. Poincaré, Nancy I, 54506 Vandoeuvre-les-Nancy, France
关键词
proton chemical-shift anisotropy; dipolar spinning sidebands;
D O I
10.1006/jmre.1997.1209
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
It is shown that the proton chemical-shift anisotropy of hydrate crystals affect dipolar powder pattern at 7.0 T. This may be clearly observed via an asymmetric envelope of dipolar spinning sidebands in magic-angle spinning proton spectra. (C) 1997 Academic Press.
引用
收藏
页码:238 / 240
页数:3
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