Microwave-assisted iodine-catalyzed oxidative coupling of dibenzyl(difurfuryl)disulfides with amines: a rapid and efficient protocol for thioamides

被引：9
|
作者：
Chen, Jinyang [1 ]
Mei, Lan [1 ]
Liu, Jialing [1 ]
Zhong, Chuntao [1 ]
Yuan, Binfang [1 ]
Li, Qiang [2 ]
机构：
[1] Yangtze Normal Univ, Coll Chem & Chem Engn, Chongqing 408000, Peoples R China
[2] Liaocheng Univ, Inst Funct Organ Mol & Mat, Sch Chem & Chem Engn, 1 Hunan St, Liaocheng 252059, Shandong, Peoples R China
来源：
RSC ADVANCES | 2019年 / 9卷 / 49期
基金：
中国国家自然科学基金;
关键词：
WILLGERODT-KINDLER REACTION; C-H THIOLATION; ORGANIC-SYNTHESIS; FUNCTIONALIZATION; BIOSYNTHESIS; CONVERSION; SYSTEMS; REAGENT; PROBES; ACIDS;
D O I：
10.1039/c9ra05939c
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
An efficient protocol for synthesis of thioamides was developed via the microwave-assisted iodine-catalyzed oxidative coupling of dibenzyl(difurfuryl)disulfides with amines. This process is scalable and tolerates a wide spectrum of amines to deliver the corresponding products in moderate to excellent yields in 10 minutes, providing a cheap and rapid approach to thioamides.
引用
收藏
页码：28576 / 28580
页数：5
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  • [2] Oxidative coupling of dibenzyl disulfide with amines catalyzed by quinoline-bromine complex: access to thioamides
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    [J]. Molecular Diversity, 2023, 27 : 159 - 165
  • [3] Oxidative coupling of dibenzyl disulfide with amines catalyzed by quinoline-bromine complex: access to thioamides
    Rezapour, Mehdi
    Abbasi, Mohammad
    [J]. MOLECULAR DIVERSITY, 2023, 27 (01) : 159 - 165
  • [4] Visible-Light-Driven Iodine-Catalyzed Synthesis of Unsymmetrical Disulfides via Oxidative Coupling
    Ren, Ming-Zhe
    Fu, Yan-Jun
    Zhang, Bo-Sheng
    Quan, Zheng-Jun
    Wang, Xi-Cun
    [J]. SYNTHESIS-STUTTGART, 2023, 55 (13): : 2011 - 2018
  • [5] Microwave-assisted oxidative coupling of amines to imines on solid acid catalysts
    Landge, Shainaz M.
    Atanassova, Valentina
    Thimmaiah, Muralidhara
    Torok, Bela
    [J]. TETRAHEDRON LETTERS, 2007, 48 (29) : 5161 - 5164
  • [6] A Rapid and Efficient Access to Polysubstituted Imidazoles via Iodine-Catalyzed Tandem Oxidative Cyclization
    Zhang Baiqun
    Wan Changfeng
    Wang Qiang
    Zhang Shuai
    Zha Zhenggen
    Wang Zhiyong
    [J]. ACTA CHIMICA SINICA, 2012, 70 (23) : 2408 - 2411
  • [7] Metal-free synthesis of sulfonamides via iodine-catalyzed oxidative coupling of sulfonyl hydrazides and amines
    Parumala, Santosh Kumar Reddy
    Peddinti, Rama Krishna
    [J]. TETRAHEDRON LETTERS, 2016, 57 (11) : 1232 - 1235
  • [8] Iodine-catalyzed sulfonylation of sulfonyl hydrazides with tert-amines: a green and efficient protocol for the synthesis of sulfonamides
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    Han, Xiaoran
    Mei, Lan
    Liu, Jinchuan
    Du, Kui
    Cao, Tuanwu
    Li, Qiang
    [J]. RSC ADVANCES, 2019, 9 (54) : 31212 - 31216
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    Wu, Yan
    Tian, Xianzhi
    Zhang, Hailing
    Chen, Rui
    Cao, Tuanwu
    [J]. CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2020, 40 (05) : 1384 - 1387
  • [10] Iodine-Catalyzed Mono- and Disulfenylation of Indoles in PEG400 through a Facile Microwave-Assisted Process
    Rahaman, Rajjakfur
    Barman, Pranjit
    [J]. EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2017, 2017 (42) : 6327 - 6334
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