Determination of trace niobium and tantalum in rock sample by atomic emission spectrometry

被引：0

作者：

Li, HZ ^{[1
]}

Zhou, CL ^{[1
]}

Luo, CN ^{[1
]}

机构：

[1] Jinan Univ, Dept Appl Chem, Jinan 250022, Peoples R China

来源：

SPECTROSCOPY AND SPECTRAL ANALYSIS | 2002年 / 22卷 / 05期

关键词：

atomic emisson spectrometry; buffer; niobium; tantalum;

D O I：

暂无

中图分类号：

O433 [光谱学];

学科分类号：

0703 ; 070302 ;

摘要：

This paper describes the determination of trace Nb and Ta in sample using carbon powder and hafnium oxide as buffer by atomic emission spectrometry (AES). Hafnium has been selected as internal standard, since it has scinilar evaporation curve as those of Nb and Ta. Samples can be I analyzed without chemical pretreatment. The sample was directly loaded. onto the ordinary electrode. The method is simple, rapid and accurate. The range of detecminiation for Nb and Ta are 0%-0.25% and 0%-0.125% respectively, and the detection limits are found to be 0.003% and 0.001%, respectively. Satisfactory results are obtained.

引用

页码：843 / 844

页数：2