Simple Catalytic Synthesis of N,N′-Dialkyl-N,N′-di(1-deoxyglucityl)ethylenediamines, Sugar-Based Gemini Surfactants

被引：0
|
作者：
Ford, Mike E. [1 ]
Kretz, C. P. [1 ]
Lassila, K. R. [1 ]
Underwood, R. P. [1 ]
Meier, I. K. [1 ]
机构：
[1] Air Prod & Chem Inc, 7201 Hamilton Blvd, Allentown, PA 18195 USA
来源：
CATALYSIS OF ORGANIC REACTIONS | 2009年 / 123卷
关键词：
D O I：
暂无
中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
Reductive coupling Of unhindered N-alkylglucamines with glyoxal in the presence of Pd/carbon provides the corresponding N,N'-dialkyl-N,N'-di(1-deoxyglucityl)ethylenediamines in good yield. Only minor amounts of byproducts are formed.
引用
收藏
页码：171 / +
页数：2
相关论文
共 50 条
  • [1] SYNTHESIS AND COORDINATION PROPERTIES OF DIALKYL-N,N-DIETHYLCARBAMYLMETHYLENEPHOSPHONATES
    BOWEN, S
    PAINE, RT
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1980, 180 (AUG): : 16 - INOR
  • [2] Synthesis and Aggregation of Novel Sugar-Based Gemini Surfactant with a N, N′-Acetylethylenediamine Spacer in Aqueous Solution
    Wang, Ruijuan
    Yan, Ruihua Wan
    Yang, Shuo
    Wang, Dong
    Yin, Zhigang
    JOURNAL OF SURFACTANTS AND DETERGENTS, 2020, 23 (04) : 697 - 703
  • [3] Synthesis of azido derivatives of N,N′-dialkyl-N,N'-dinitro-methanediamines and ternary mixtures based thereon
    Sigai, N. V.
    Serkov, S. A.
    Ermakov, A. S.
    Tartakovskii, V. A.
    Luk'yanov, O. A.
    Ternikova, T. V.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2007, 43 (03) : 458 - 460
  • [4] Synthesis of azido derivatives of N,N′-dialkyl-N,N′-dinitro-methanediamines and ternary mixtures based thereon
    N. V. Sigai
    S. A. Serkov
    A. S. Ermakov
    V. A. Tartakovskii
    O. A. Luk’yanov
    T. V. Ternikova
    Russian Journal of Organic Chemistry, 2007, 43 : 458 - 460
  • [5] Efficient synthesis of N,N′-dialkyl-N"-dialkylaminocarbothioyl thioureas from cyclic secondary amines, CS2, and N,N′-dialkyl carbodiimides in water
    Yavari, Issa
    Hosseini, Nargess
    Moradi, Loghman
    Mirzaei, Anvar
    TETRAHEDRON LETTERS, 2008, 49 (27) : 4239 - 4241
  • [6] Adsorption and aggregation properties of amino acid-based N-alkyl cysteine monomeric and N,N′-dialkyl cystine gemini surfactants
    Yoshimura, Tomokazu
    Sakato, Ayako
    Tsuchiya, Koji
    Ohkubo, Takahiro
    Sakai, Hideki
    Abe, Masahiko
    Esumi, Kunio
    JOURNAL OF COLLOID AND INTERFACE SCIENCE, 2007, 308 (02) : 466 - 473
  • [7] SIMPLE SYNTHESIS OF N,N-DIALKYL-3-ALKEN-1-YN-1-AMINES
    VERBOOM, W
    EVERHARDUS, RH
    BOS, HJT
    BRANDSMA, L
    RECUEIL DES TRAVAUX CHIMIQUES DES PAYS-BAS-JOURNAL OF THE ROYAL NETHERLANDS CHEMICAL SOCIETY, 1979, 98 (10): : 508 - 511
  • [8] SYNTHESIS OF N,N'-DIACYL-1,2-DI-(4-PYRIDYL)ETHYLENEDIAMINES
    BRANA, MF
    RODRIGUEZ, MLL
    GARRIDO, J
    ROLDAN, CM
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 1981, 18 (07) : 1305 - 1308
  • [9] IMPROVEMENT IN THE SYNTHESIS OF N,N'-DIACYL-1,2-DI(4-PYRIDYL)ETHYLENEDIAMINES
    BRANA, MF
    CASTELLANO, JM
    RODRIGUEZ, MLL
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 1983, 20 (06) : 1723 - 1724
  • [10] Syntheses and antitumor activities of N′1,N′3-dialkyl-N′1,N′3-di-(alkylcarbonothioyl) malonohydrazide: The discovery of elesclomol
    Chen, Shoujun
    Sun, Lijun
    Koya, Keizo
    Tatsuta, Noriaki
    Xia, Zhiqiang
    Korbut, Timothy
    Du, Zhenjian
    Wu, Jim
    Liang, Guiqing
    Jiang, Jun
    Ono, Mitsunori
    Zhou, Dan
    Sonderfan, Andrew
    BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 2013, 23 (18) : 5070 - 5076
12345