Using the electrochemical quartz crystal microbalance as stripping detector. Application to trace mercury analysis

被引：0
|
作者：
Andersen, NPR [1 ]
HolstHansen, P [1 ]
Britz, D [1 ]
机构：
[1] AARHUS UNIV,DEPT CHEM,DK-8000 AARHUS C,DENMARK
来源：
ANALYTICA CHIMICA ACTA | 1996年 / 329卷 / 03期
关键词：
quartz crystal microbalance; mercury;
D O I：
暂无
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
The electrochemical quartz crystal microbalance (EQCM) was used as a stripping detector for mercury(II) in 0.1 M perchloric acid with a plating time of 15 min. Mercury concentrations down to 1 ppb could be measured. The calibration curve, stripping frequency change vs. mercury(II) concentration, showed nonlinearity at mercury(II) concentrations higher than 75 ppb. Kinetic and experimental factors appear to be the cause.
引用
收藏
页码：253 / 256
页数：4
相关论文
共 50 条
  • [1] Using the electrochemical quartz crystal microbalance as stripping detector. Application to trace mercury analysis
    Anal Chimica Acta, 3 (253):
  • [2] Application of Electrochemical Quartz Crystal Microbalance
    Wei, Xiaoyan
    Wang, Gang
    Li, Anfeng
    Quan, Yizhou
    Chen, Jinwei
    Wang, Ruilin
    PROGRESS IN CHEMISTRY, 2018, 30 (11) : 1701 - 1721
  • [3] Limitations of the use of the electrochemical quartz crystal microbalance in stripping analysis of lead(II) and cadmium(II) on a quartz crystal platinum electrode with a thin mercury film
    Andersen, NPR
    ANALYTICA CHIMICA ACTA, 1998, 368 (03) : 191 - 196
  • [4] Stable mercury films on gold for the electrochemical quartz crystal microbalance
    Cho, KC
    Yoon, S
    Jung, MC
    Kim, H
    COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS, 1998, 134 (1-2) : 59 - 65
  • [5] Development of chloroorganics detector using quartz crystal microbalance
    Noda, K
    Naganawa, R
    Tao, H
    IECON '98 - PROCEEDINGS OF THE 24TH ANNUAL CONFERENCE OF THE IEEE INDUSTRIAL ELECTRONICS SOCIETY, VOLS 1-4, 1998, : 1220 - 1225
  • [6] Stable mercury and carbon films on gold for electrochemical quartz crystal microbalance
    Yoon, S
    Jung, MC
    Cho, K
    Kim, H
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1996, 212 : 80 - COLL
  • [7] Electrochemical study of methylalkylviologens using an electrochemical quartz crystal microbalance
    Lee, C
    Lee, YK
    Lee, Y
    Jeon, IC
    JOURNAL OF ELECTROANALYTICAL CHEMISTRY, 1999, 463 (02): : 224 - 231
  • [8] Observation of Mercury Underpotential Deposition on an Ir Surface using the Electrochemical Quartz Crystal Microbalance Technique
    Nagai, Tsukasa
    Siroma, Zyun
    Akita, Tomoki
    Ioroi, Tsutomu
    ELECTROANALYSIS, 2022, 34 (09) : 1381 - 1386
  • [9] Electrochemical printing:: in situ characterization using an electrochemical quartz crystal microbalance
    Nelson, JB
    Schwartz, DT
    JOURNAL OF MICROMECHANICS AND MICROENGINEERING, 2005, 15 (12) : 2479 - 2484
  • [10] ELECTROCHEMICAL APPLICATIONS OF THE QUARTZ CRYSTAL MICROBALANCE
    DEAKIN, MR
    BUTTRY, DA
    ANALYTICAL CHEMISTRY, 1989, 61 (20) : A1147 - +
12345