Crystal structure of aqua-bis(acrylato-O,O′)(1,10-phenanthroline-N,N′)zinc(II) hydrate, Zn(C3H3O2)2(H2O)(C12H10N2) • H2O

被引：0
|
作者：
Deng, Q. [1 ]
Jiang, W-J. [1 ]
Peng, Z. -S. [1 ]
Long, Y. -F. [1 ]
Cai, T-J. [1 ]
机构：
[1] Hunan Univ Sci & Technol, Coll Chem & Chem Engn, Xiangtan 411201, Hunan, Peoples R China
来源：
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2006年 / 221卷 / 03期
关键词：
D O I：
10.1524/ncrs.2006.0077
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
A mixture solution of 18 ml H2O/ethanol (1:1, v/v) containing ZnO (0.0814 g, 1.0 mmol), 1,10-phenanthroline monohydrate (0.198 g, 1.0 mmol) and acrylic acid (0.144 g, 2.0 mmol) was sealed in a Teflon-lined stainless steel vessel (25 ml), and the vessel was heated at 363 K for 7d, then cooled to room temperature and filtered off. The resultant filtrate was allowed to stand by slow evaporation at room temperature. The colorless block crystals generated 21 days later (yield 50 % based on the initial ZnO input).
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页码：287 / 288
页数：2
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