A microwave-assisted solvent- and catalyst-free synthesis of aminomethylene bisphosphonates

被引：28
|
作者：
Kaboudin, Babak [1 ]
Alipour, Soheil [1 ]
机构：
[1] IASBS, Dept Chem, Gava Zang 451951159, Zanjan, Iran
来源：
TETRAHEDRON LETTERS | 2009年 / 50卷 / 29期
关键词：
ALPHA-AMINO PHOSPHONATES; ONE-POT SYNTHESIS; ORGANIC PHOSPHORUS-COMPOUNDS; AMMONIUM HYDROGEN CARBONATE; CONVENIENT SYNTHESIS; DIASTEREOSELECTIVE SYNTHESIS; AMINOPHOSPHONIC ACIDS; BIOLOGICAL-ACTIVITY; TRYPANOSOMA-BRUCEI; PHOSPHINIC ACIDS;
D O I：
10.1016/j.tetlet.2009.05.016
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A convenient preparative approach for the synthesis of aminomethylene bisphosphonates is developed which involves treatment of amines with triethyl orthoformate and diethyl phosphite under microwave irradiation. (C) 2009 Elsevier Ltd. All rights reserved.
引用
收藏
页码：4243 / 4245
页数：3
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