The 2:1 complex of maleic acid and 1,4-diazabicyclo[2.2.2]octane:: hydrogen-bonded sheets linked by C-H•••O hydrogen bonds

被引：11
|
作者：
Sun, CR
Jin, ZM [1 ]
机构：
[1] Zhejiang Univ Technol, Coll Pharmaceut Sci, Hangzhou 310014, Peoples R China
[2] Zhejiang Univ, Dept Chem, Hangzhou 310027, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 2002年 / 58卷
关键词：
D O I：
10.1107/S0108270102014956
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
In the title complex, 1,4-diazoniabicyclo[2.2.2]octane bis(hydrogen maleate), C6H14N22+.2C(4)H(3)O(4)(-), the C4H3O4- and C6H14N22+ ions, derived from maleic acid and 1,4-diazabicyclo[2.2.2]octane, respectively, are disordered across a mirror plane in space group Cmc2(1), and they are linked by two nearly linear N-H...O hydrogen bonds, with N...O distances of 2.662 (3) and 2.614 (4) Angstrom, and N-H...O angles of 173degrees. The crystal structure consists of sheets with reticulations of 3.3792 (4) Angstrom in stratum and 7.3892 (8) Angstrom in width. The sheets are linked by C-H...O hydrogen bonds.
引用
收藏
页码：O600 / O601
页数：2
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