Ball milling effect on the structure of single-wall carbon nanotubes

被引:162
|
作者
Pierard, N
Fonseca, A
Colomer, JF
Bossuot, C
Benoit, JM
Van Tendeloo, G
Pirard, JP
Nagy, JB
机构
[1] Fac Univ Notre Dame Paix, Lab Resonance Magnet Nucl, B-5000 Namur, Belgium
[2] Univ Antwerp, RUCA, EMAT, B-2020 Antwerp, Belgium
[3] Univ Liege, Lab Genie Chim, B-4000 Liege, Belgium
[4] Max Planck Inst Solid State Res, D-70569 Stuttgart, Germany
[5] LPC, Inst Mat Jean Rouxel, F-44322 Nantes 3, France
关键词
carbon nanotubes; grinding; fracture; mechanical properties; surface areas;
D O I
10.1016/j.carbon.2004.02.031
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
The vibratory mill is used to decrease the single-wall carbon nanotubes (SWNTs) length and to increase their specific surface area. Electron microscopy, Raman spectroscopy, X-ray diffraction and BET measurements indicated that the optimum time of treatment seems to be 2 h. After that, the SWNTs quality decreases, with a complete disruption of the tubular structure leading to multi-layered polyaromatic carbon materials observed after 50 h. (C) 2004 Elsevier Ltd. All rights reserved.
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页码:1691 / 1697
页数:7
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