N,N-Bis(2,6-difluorobenzyl)-1,3,4-thiadiazol-2-amine

被引:0
|
作者
Fun, Hoong-Kun [1 ]
Liew, Wei-Ching [1 ]
Chandrakantha, B. [2 ]
Isloor, Arun M. [3 ]
机构
[1] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, George Town 11800, Malaysia
[2] Syngene Int Ltd, Bangalore 560100, Karnataka, India
[3] Natl Inst & Technol Karnataka, Dept Chem, Mangalore 575025, India
关键词
DERIVATIVES;
D O I
10.1107/S1600536809031675
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C16H11F4N3S, the dihedral angles between the thiadiazole ring and the difluorobenzyl rings are 81.95 (7) and 81.96 (7)degrees, whereas the dihedral angle between the difluorobenzyl rings is 11.41 (7)degrees. In the crystal structure, C-H center dot center dot center dot N and C-H center dot center dot center dot F interactions link the molecules into two-dimensional arrays parallel to the bc plane.
引用
收藏
页码:O2166 / U2134
页数:11
相关论文
共 50 条
  • [1] 5-(2,6-Difluorophenyl)-1,3,4-thiadiazol-2-amine
    Wang, Yao
    Wan, Rong
    Han, Feng
    Wang, Peng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O3108 - U735
  • [2] Cyclocondensation of 1,3,4-thiadiazol-2-amine with β-sulfonylvinyltrifluoromethyldiols
    Krasovsky, AL
    Moiseev, AM
    Nenajdenko, VG
    Balenkova, ES
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 2002, (02): : 253 - 260
  • [3] 5,5′-[methylenebis(sulfanediyl)]bis(1,3,4-thiadiazol-2-amine)
    Meng, Fankun
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O2000 - U4451
  • [4] N-[Phenyl(piperidin-1-yl)methyl]-1,3,4-thiadiazol-2-amine
    Liu, Juan
    Deng, Yu-Heng
    Li, Pei-Zhou
    Jin, Qiong-Hua
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O4849 - U6364
  • [5] Synthesis and crystal structure of N-butyl-5-(4-methyl-1,2,3-thiadiazol-5-yl)-1,3,4-thiadiazol-2-amine and 5-isoquinolin-3-yl-N-(2-methylphenyl)-1,3,4-thiadiazol-2-amine
    Wawrzycka-Gorczyca, Irena
    Siwek, Agata
    Kosikowska, Urszula
    Malm, Anna
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-CRYSTALLINE MATERIALS, 2011, 226 (03): : 297 - 302
  • [7] 5-(Adamantan-1-yl)-N-methyl-1,3,4-thiadiazol-2-amine
    Al-Tamimi, Abdul-Malek S.
    Alafeefy, Ahmed M.
    El-Emam, Ali A.
    Ng, Seik Weng
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O683 - +
  • [8] 5-(2-Methylphenyl)-1,3,4-thiadiazol-2-amine
    Wang, Yao
    Kong, Xiang-Jun
    Wan, Rong
    Han, Feng
    Wang, Peng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O961 - U1489
  • [9] 5-(2-bromophenyl)-1,3,4-thiadiazol-2-amine
    Yin, Li-He
    Wan, Rong
    Wang, Yao
    Han, Feng
    Wang, Jin-Tang
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1884 - U3391
  • [10] 2-(4-Fluorobenzylidene)-N-(4-methoxybenzylidene)-1,3,4-thiadiazol-2-amine
    He, Qiu
    An, Kang
    Wang, Peng
    Yu, Peng
    Wan, Rong
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1716 - U672