Polycyclic aromatic hydrocarbons in edible oils: analysis by molecularly imprinted solid-phase extraction with HPLC-FLD

被引：0
|
作者：
Yu, Ye [1 ,2 ,3 ,4 ]
Wang, Yue [2 ]
Jin, Qinze [1 ,3 ,4 ]
Dong, Hua [5 ]
Wang, Xingguo [1 ,3 ,4 ]
机构：
[1] Jiangnan Univ, State Key Lab Food Sci & Technol, Wuxi 214122, Peoples R China
[2] Food Inspect Author Zhangjiagang Entry Exit Inspe, Zhangjiagang 215600, Peoples R China
[3] Jiangnan Univ, Sch Food, Wuxi 214122, Peoples R China
[4] Synerget Innovat Ctr Food Safety & Nutr, Wuxi 214122, Peoples R China
[5] Eastocean Oils & Grains Ind Zhangjiagang CO LTD, Zhangjiagang 215634, Peoples R China
来源：
AGRO FOOD INDUSTRY HI-TECH | 2014年 / 25卷 / 03期
基金：
国科技部“十一五”科技计划项目;
关键词：
polycyclic aromatic hydrocarbons; HPLC-FLD; fats; vegetable oils; molecularly imprinted solid-phase extraction; CHROMATOGRAPHY-MASS SPECTROMETRY; SAMPLES; SPAIN; FATS; FOOD; PAH;
D O I：
暂无
中图分类号：
Q81 [生物工程学（生物技术）]; Q93 [微生物学];
学科分类号：
071005 ; 0836 ; 090102 ; 100705 ;
摘要：
A new method was developed to determine the presence of polycyclic aromatic hydrocarbons (PAHs) in edible fats and oils. Samples are dissolved in petroleum ether, and PAHs are adsorbed onto a molecularly imprinted solid-phase extraction (MIPSPE) cartridge and eluted with ethyl acetate. After evaporation of the solvent, PAHs were re-dissolved in acetonitrile and analyzed by RP-HPLC with fluorescence detection. The detection limits of PAHs were 0.04-0.66 mu g/kg and the recovery rates ranged from 56.0 percent to 109.1 percent. The total contents of PAHs in edible oils were 18.00-639.96 mu g/kg. The developed method was effective due to its high specificity for PAHs.
引用
收藏
页码：19 / 22
页数：4
相关论文
共 50 条
  • [1] Determination of polycyclic aromatic hydrocarbons in coffee and tea samples by magnetic solid-phase extraction coupled with HPLC-FLD
    Shi, Yating
    Wu, Hao
    Wang, Chaoqiong
    Guo, Xiaozhen
    Du, Juanli
    Du, Liming
    [J]. FOOD CHEMISTRY, 2016, 199 : 75 - 80
  • [2] Method Validation and Determination of Polycyclic Aromatic Hydrocarbons in Vegetable Oils by HPLC-FLD
    Alicja Zachara
    Dorota Gałkowska
    Lesław Juszczak
    [J]. Food Analytical Methods, 2017, 10 : 1078 - 1086
  • [3] Method Validation and Determination of Polycyclic Aromatic Hydrocarbons in Vegetable Oils by HPLC-FLD
    Zachara, Alicja
    Galkowska, Dorota
    Juszczak, Lesaw
    [J]. FOOD ANALYTICAL METHODS, 2017, 10 (04) : 1078 - 1086
  • [4] Polycyclic aromatic hydrocarbons in teas using QuEChERS and HPLC-FLD
    Tfouni, Silvia A. V.
    Reis, Raquel M.
    Kamikata, Kamille
    Gomes, Fernanda M. L.
    Morgano, Marcelo A.
    Furlani, Regina P. Z.
    [J]. FOOD ADDITIVES & CONTAMINANTS PART B-SURVEILLANCE, 2018, 11 (02): : 146 - 152
  • [5] Automated solid-phase extraction coupled online with HPLC-FLD for the quantification of zearalenone in edible oil
    Drzymala, Sarah S.
    Weiz, Stefan
    Heinze, Julia
    Marten, Silvia
    Prinz, Carsten
    Zimathies, Annett
    Garbe, Leif-Alexander
    Koch, Matthias
    [J]. ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2015, 407 (12) : 3489 - 3497
  • [6] Automated solid-phase extraction coupled online with HPLC-FLD for the quantification of zearalenone in edible oil
    Sarah S. Drzymala
    Stefan Weiz
    Julia Heinze
    Silvia Marten
    Carsten Prinz
    Annett Zimathies
    Leif-Alexander Garbe
    Matthias Koch
    [J]. Analytical and Bioanalytical Chemistry, 2015, 407 : 3489 - 3497
  • [7] HPLC-FLD Simultaneous Determination of 13 Polycyclic Aromatic Hydrocarbons: Validation of an Analytical Procedure for Soybean Oils
    Camargo, Monica C. R.
    Antoniolli, Paula R.
    Vicente, Eduardo
    [J]. JOURNAL OF THE BRAZILIAN CHEMICAL SOCIETY, 2011, 22 (07) : 1354 - 1361
  • [8] Monitoring Seasonal Differences on Contamination and Carry-over of Zearalenone from Feedstuffs to Foods by Molecularly Imprinted Solid-phase Extraction and HPLC-FLD
    Ya-ting Wu
    Chang-gang Huang
    Ning Li
    Jun-feng Qi
    Yi-Yang Guo
    Bin Lu
    [J]. Food Analytical Methods, 2022, 15 : 448 - 457
  • [9] Monitoring Seasonal Differences on Contamination and Carry-over of Zearalenone from Feedstuffs to Foods by Molecularly Imprinted Solid-phase Extraction and HPLC-FLD
    Wu, Ya-ting
    Huang, Chang-gang
    Li, Ning
    Qi, Jun-feng
    Guo, Yi-Yang
    Lu, Bin
    [J]. FOOD ANALYTICAL METHODS, 2022, 15 (02) : 448 - 457
  • [10] Determination of polycyclic aromatic hydrocarbons in aqueous samples using recycled polystyrene for pipette tip-solid phase extraction followed by HPLC-FLD
    Lopez-Tellez, Jorge
    Rodriguez, Jose A.
    Miranda, Jose M.
    Mondragon, Alicia C.
    Ibarra, Israel S.
    [J]. INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 2022,
12345