A novel synthetic route to layered double hydroxides using hexamethylenetetramine

被引:142
|
作者
Iyi, N [1 ]
Matsumoto, T [1 ]
Kaneko, Y [1 ]
Kitamura, K [1 ]
机构
[1] NIMS, Adv Mat Lab, Tsukuba, Ibaraki 3050044, Japan
关键词
D O I
10.1246/cl.2004.1122
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
For the homogeneous precipitation of hydrotalcite-like compounds (layered double hydroxides; LDHs), HMT (hexamethylenetetramine) was used and the conditions for obtaining the LDHs were investigated. The well-crystallized 1-5 mum LDHs were obtained in a pressure vessel after a 1-day treatment at 140 degreesC. The resulting LDHs contained a carbonate anion, which was successfully deintercalated using an NaCl-HCI mixed solution without any morphological change.
引用
收藏
页码:1122 / 1123
页数:2
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