Crystal and molecular structure of N,N,N′,N′-tetra(2-nitrilethyl) ethane-1,2-diamine and N-(2-nitrilethyl)benzylamine hydrobromide

被引：1

作者：

Gao, J. ^{[1
]}

Xu, X. -Y. ^{[1
]}

Xu, T. -T. ^{[1
]}

Ni, J. ^{[1
]}

Liu, Q. -L. ^{[1
]}

机构：

[1] Univ Sci & Technol China, Dept Chem, Wuhan, Peoples R China

来源：

JOURNAL OF STRUCTURAL CHEMISTRY | 2006年 / 47卷 / 02期

关键词：

N,N,N ',N '-tetra(2-nitrilethyl) ethane-1,2-diamine; N-(2-nitrilethyl)benzylamine hydrobromide; structure of molecular crystals;

D O I：

10.1007/s10947-006-0312-x

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

N,N,N',N'-tetra(2-nitrilethyl) ethane-1,2-diamine and N-(2-nitrilethyl)benzylamine hydrobromide were prepared by the addition reaction of acrylonitrile with corresponding amines, and the two structures were determined by X-ray single crystal diffraction. The two compounds crystallize in monoclinic system, and almost no classical hydrogen bond exists in the two crystal structures.

引用

页码：383 / 386

页数：4

共 50 条

[1] Crystal and molecular structure of N,N,N′,N′-tetra(2-nitrilethyl) ethane-1,2-diamine and N-(2-nitrilethyl)benzylamine hydrobromide
J. Gao
X.-Y. Xu
T.-T. Xu
J. Ni
Q.-L. Liu
Journal of Structural Chemistry, 2006, 47 : 383 - 386
[2] CRYSTAL-STRUCTURE OF N,N,N',N'-TETRAKIS-(TRIMETHYLSILYL)ETHANE-1,2-DIAMINE
ENGELHARDT, LM
RASTON, CL
WHITE, AH
AUSTRALIAN JOURNAL OF CHEMISTRY, 1985, 38 (11) : 1729 - 1733
[3] N,N′-bis(2-thienylmethylene)ethane-1,2-diamine
Wang, Da-Qi
Wang, Qiang
Xiao, Li-Jun
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O4865 - U6525
[4] N,N′-Bis(2-aminobenzyl)ethane-1,2-diamine
de Barbarin, Cecilia Rodriguez
Bernes, Sylvain
Najera, Blanca
Elizondo, Perla
Cerda, Patricia
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O549 - O550
[5] N,N'-bis(2-iodobenzylidene)ethane-1,2-diamine
Fun, Hoong-Kun
Kia, Reza
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1870 - U3288
[6] N,N′-Bis(2,3-dimethoxybenzylidene)ethane-1,2-diamine
Xue, Hua
Li, Wenjuan
Han, Hongfei
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2431 - U1148
[7] N,N′-bis[(E)-2-benzylidenepropylidene]ethane-1,2-diamine
Khalaji, Aliakbar Dehno
Ng, Seik Weng
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1771 - U2078
[8] [μ-N,N′-Bis(2-pyridylmethylene)ethane-1,2-diamine]bis{aqua[N,N′-bis(2-pyridylmethylene)ethane-1,2-diamine]manganese(II)} tetrakis(perchlorate)
Ha, Kwang
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M255 - U3139
[9] [N,N-Bis(2-aminoethyl)ethane-1,2-diamine](ethane-1,2-diamine)nickel(II) thiosulfate trihydrate
Seidlhofer, Beatrix
Nather, Christian
Bensch, Wolfgang
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 : M167 - U826
[10] [N,N′-Dimethyl-N"-(2-pyridylmethylene)-ethane-1,2-diamine]dithiocyanatozinc(II)
Chen, G
Bai, ZP
Qu, SJ
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : M2483 - M2484

← 1 2 3 4 5 →