NEW HYBRID COMPOUNDS CONTAINING INTERCALATED CIPROFLOXACIN INTO LAYERED DOUBLE HYDROXIDES: SYNTHESIS AND CHARACTERIZATION

被引：0
|
作者：
Silion , Mihaela [1 ]
Popa, Marcel Ionel [1 ]
Lisa, Gabriela [1 ]
Hritcu, Doina [1 ]
机构：
[1] Iasi Tech Univ, Fac Chem Engn & Environm Protect, Iasi 700050, Romania
来源：
REVUE ROUMAINE DE CHIMIE | 2008年 / 53卷 / 09期
关键词：
layered double hydroxides; ciprofloxacin; coprecipitation; ion exchange;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
This work presents the synthesis, physical and chemical characterization of layered double hydroxides containing Zn and Al (ZnAlLDH) intercalated with ciprofloxacin (CFX) (1-cyclopi-opyl-6-fluoro-1,4-dillydi-o-4-oxo-7-(1-piperazinyl)-3-quinoline carboxylic acid). The products were prepared by two different techniques: coprecipitation and ion exchange. The hybrid materials were studied by X-ray diffraction (XRD), FTIR spectroscopy and thermogravimetry. The results of the XRD analysis confirm that all the products present (lie crystalline structure characteristic for hydrotalcite-like compounds. The FTIR and TG-DTG analyses confirm the intercalation of the organic compound within the hydrotalcite matrix.
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页码：827 / +
页数：6
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