Synthesis of benzo[a]furo[2, 3-c]phenazine derivatives through an efficient, rapid and via microwave irradiation under solvent-free conditions catalyzed by H3PW12O40@Fe3O4-ZnO for high-performance removal of methylene blue

被引:15
|
作者
Taheri, Milad [1 ]
Mohebat, Razieh [1 ]
Moslemin, Mohammad Hossein [1 ]
机构
[1] Islamic Azad Univ, Yazd Branch, Dept Chem, Yazd, Iran
关键词
Multi-component; magnetic core-shell nanoparticles; microwave-assisted; solvent-free conditions; green synthesis; PHOTOCATALYTIC DEGRADATION; NANOPARTICLES; HETEROSTRUCTURES; NANOCATALYST; FABRICATION; ACID; IRON;
D O I
10.1080/21691401.2021.1894163
中图分类号
Q81 [生物工程学(生物技术)]; Q93 [微生物学];
学科分类号
071005 ; 0836 ; 090102 ; 100705 ;
摘要
A rapid, one-pot synthesis of eight benzo[a]furo[2,3-c]phenazine derivatives has been achieved in moderate to good yields in good yields via a multi-component of 2-hydroxynaphthalene-1,4-dione, arylglyoxal, indole (H, CH3) in the presence of H3PW12O40@Fe3O4-ZnO magnetic core-shell nanoparticles (MCNPs) under solvent-free conditions using microwave irradiation. The catalyst was synthesised and characterised by X-ray diffraction, EDX, TEM, FESEM, TGA, VSM and atomic force microscope. As an application for the synthesised nanocatalyst, degradation of methylene blue as heavy-mass organic pollution was measured. These results showed advantages for synthesis, such as mild reaction conditions, low energy consumption and economically affordable.
引用
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页码:250 / 260
页数:11
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