International Key Comparison CCQM-K94 (10 μmol/mol Dimethyl sulfide in nitrogen)

被引:5
|
作者
Lee, Sangil [1 ]
Heo, Gwi Suk [1 ]
Kim, Yongdoo [1 ]
Oh, Sanghyub [1 ]
Han, Qiao [2 ]
Wu, Hai [2 ]
Konopelko, L. A. [3 ]
Kustikov, Y. A. [3 ]
Kolobova, A. V. [3 ]
Efremova, O. V. [3 ]
Pankratov, V. V. [3 ]
Pavlov, M. V. [3 ]
Culleton, Lucy P. [4 ]
Brown, Andrew S. [4 ]
Brookes, Chris [4 ]
Li, Jianrong [5 ]
Ziel, Paul R. [5 ]
van der Veen, Adriaan M. H. [5 ]
机构
[1] Korea Res Inst Stand & Sci, Ctr Gas Anal, 267 Gajeong Ro, Daejeon 305340, South Korea
[2] Natl Inst Metrol NIM China, 18 Bei San Huan Dong Str, Beijing 100013, Peoples R China
[3] DI Mendeleyev Inst Metrol VNIIM, Res Dept State Measurement Stand Field Physicoche, 19 Moskovsky Prospekt, St Petersburg 198005, Russia
[4] Natl Phys Lab, Hampton Rd, Teddington TW11 0LW, Middx, England
[5] VSL, Thijsseweg 11, NL-2629 JA Delft, Netherlands
关键词
Gas mixtures;
D O I
10.1088/0026-1394/53/1A/08002
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
The purpose of the international key comparison CCQM-K94 was to compare the measurement capability of dimethyl sulfide (DMS) at approximately 10 mmol/mol and expectation to contribute the establishment of traceability to single measurement scale for DMS between NMIs. A total of 8 primary standard gas mixtures (PSMs), including DMS in nitrogen with a nominal amount-of-substance fraction of about 10 μmol/mol, was prepared gravimetrically through a two-step dilution process and verified with gas chromatography/flame ionization detector (GC/FID). The amount-of-substance fractions determined by the gravimetric preparation were adopted as key comparison reference values (KCRVs). The PSMs were compared against a reference gas mixture for their verification.
引用
收藏
页码:1 / 28
页数:28
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