Synthesis and structure of bis[1-(1-adamantyl)-4,4,4-trifluorobutane-2,4-dionato]copper

被引：3
|
作者：
Khamylov, V. K. [1 ]
Pochekutova, T. S. [1 ]
Petrov, B. I. [1 ]
Sizov, M. V. [1 ]
Fukin, G. K. [1 ]
Kurskii, Yu. A. [1 ]
Arapova, A. V. [1 ]
机构：
[1] Russian Acad Sci, Razuvaev Inst Organomet Chem, Nizhnii Novgorod 603600, Russia
来源：
RUSSIAN JOURNAL OF GENERAL CHEMISTRY | 2009年 / 79卷 / 01期
基金：
俄罗斯基础研究基金会;
关键词：
COMPLEXES;
D O I：
10.1134/S1070363209010058
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Previously unknown 1-(1-adamantyl)-4,4,4-trifluorobutane-2,4-dione and its copper complex, bis [1-(1-adamantyl)-4,4,4-trifluorobutane-2,4-dionato]copper, were synthesized. The (1)H NMR, IR, and ESR spectra and X-ray diffraction patterns of the synthesized compounds were obtained. Volatilily and thermal stability of the copper complex were studied by thermogravimetric analysis and differential scanning calorimetry.
引用
收藏
页码：31 / 36
页数：6
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