Room temperature route to phosphorus nitride hollow spheres

被引：5
|
作者：
Chen, LY [1 ]
Gu, YL [1 ]
Shi, L [1 ]
Yang, ZH [1 ]
Ma, JH [1 ]
Qian, YT [1 ]
机构：
[1] Univ Sci & Technol China, Dept Chem, Struct Res Lab, Hefei 230026, Anhui, Peoples R China
来源：
INORGANIC CHEMISTRY COMMUNICATIONS | 2004年 / 7卷 / 05期
关键词：
phosphorus nitride; X-ray powder diffraction; chemical synthesis;
D O I：
10.1016/j.inoche.2004.03.009
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Amorphous phosphorus nitride (P3N5) hollow spheres were synthesized via reacting PCl3 with NaNH2 at room temperature. Transmission electron microscopy (TEM) images showed the hollow spheres with a diameter of 80-150 nm. X-ray photoelectron spectra (XPS) were used to determine the molar ratio of 1:1.60 for P:N. The optical properties of the as-prepared P3N5 were investigated. (C) 2004 Published by Elsevier B.V.
引用
收藏
页码：643 / 645
页数：3
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