Synthesis and Crystal Structure of a New Zinc(II) Coordination Polymer Assembled by 4-Nitrophthalic Acid and Bis(imidazol) Ligands

被引：0
|
作者：
Xing Zheng [1 ]
Wang Qing-Wei [2 ]
Sui Wei [2 ]
Liu Bo [2 ]
机构：
[1] Zhenjiang Coll, Dept Chem Engn, Zhenjiang 212000, Jiangsu, Peoples R China
[2] Jilin Normal Univ, Minist Educ, Key Lab Preparat & Applicat Environm Friendly Mat, Siping 136000, Jilin, Peoples R China
来源：
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY | 2018年 / 37卷 / 01期
关键词：
Zn(II) coordination polymer; bis(imidazole) ligand; luminescent property; synthesis; ORGANIC FRAMEWORKS; COMPLEXES; TEMPERATURE; SORPTION; ZEOLITE; NETWORK; FE(II); GAS; 2D; NI;
D O I：
10.14102/j.cnki.0254-5861.2011-1669
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A new complex [Zn(4-nph)(bib)](2n)center dot nH(2)O (1) has been obtained by the reaction of metal (Zn(II)), 1,4-bis(imidazol-1-yl)-butane (bib) with 4-nitrophthalic acid (4-H(2)nph). The crystal structure of 1 has been determined by single-crystal X-ray diffraction analysis. Compound 1 is of triclinic system, space group P (1) over bar with a = 10.3251, b = 12.4503, c = 16.6497 angstrom, alpha = 88.487(3), beta = 72.529(3), gamma = 79.991(3)degrees, V = 2009.8(5) angstrom(3) and M-r = 945.47. Complex 1 shows a three-dimensional (3D) framework. Moreover, through intermolecular hydrogen bonds, compound 1 is assembled into a supramolecular structure. The thermal stability and luminescent properties of 1 are also investigated.
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页码：125 / 130
页数：6
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