Precursor induced evolution in single anatase phase synthesis of TiO2 nanoparticles for water treatment and dye-sensitized solar cell

被引:17
|
作者
Keshari, Ashish Kumar [1 ]
Choudhary, Preeti [1 ]
Shukla, Vivek Kumar [1 ]
机构
[1] Gautam Buddha Univ, Dept Appl Phys, Greater Noida 201312, India
关键词
TiO2; TTIP; TiCl4; Sol-gel; Water-treatment; DSSC; TITANIUM-DIOXIDE NANOPARTICLES; NANOCRYSTALS;
D O I
10.1016/j.physb.2022.413716
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
TiO2 nanoparticles (NPs) have been synthesized by employing the pure and special sol-gel approach with different precursors viz. micro-sized TiO2 powder, TiCl4 (Titanium tetrachloride) and TTIP (Titanium isoprop-oxide). The synthesized NPs were characterized by X-ray diffraction (XRD), Field emission-scanning electron microscopy (FESEM), UV-Vis spectrographic analysis and Photoluminescence spectrographic analysis. The XRD results show single anatase phase for all the precursor-based samples. The characterizations results lead to originate that the TiCl4 precursor based TiO2 NPs are the finest NPs with admirable results. No phase trans-formation was observed in micro-sized TiO2 precursor-based NPs even after annealed at various temperatures (300 ?degrees C, 600 ?degrees C, and 900 ?degrees C). The TiCl4 precursor-based NPs were used for water treatment with UV radiation exposure and treated water samples were analysed with UV-visible spectrographic technique. Further, micro-sized and TiCl4 precursor based TiO2 NPs were also used in fabricating dye-sensitized solar cell (DSSC).
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页数:9
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