Determination of Polycyclic Aromatic Hydrocarbons in Mosses by Ultrasonic-Assisted Extraction and Gas Chromatography-Tandem Mass Spectrometry

被引：1
|
作者：
Wu, Rangtian [1 ]
Li, Na [1 ,2 ]
Shu, Rong [1 ]
An, Na [1 ]
Yi, Feng [1 ]
Yang, Wei [2 ]
Li, Chongying [1 ]
机构：
[1] Chengdu Univ Technol, Mineral Resources Chem Key Lab Sichuan Higher Edu, Coll Mat & Chem & Chem Engn, Chengdu, Peoples R China
[2] Chengdu Univ Technol, State Key Lab Oil & Gas Reservoir Geol & Exploita, Coll Energy Resource, Chengdu, Peoples R China
来源：
ANALYTICAL LETTERS | 2017年 / 50卷 / 01期
基金：
中国国家自然科学基金;
关键词：
Gas chromatography-tandem mass spectrometry; mosses; polycyclic aromatic hydrocarbons; ultrasonic-assisted extraction; SCHREBERI BRID. MITT; SPLENDENS HEDW. BSG; SOUTH-CENTRAL POLAND; ATMOSPHERIC DEPOSITION; SPATIAL-DISTRIBUTION; PAH CONCENTRATIONS; LIQUID-EXTRACTION; TRACE-ELEMENTS; PINE NEEDLES; POLLUTION;
D O I：
10.1080/00032719.2016.1166371
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A facile method for the determination of polycyclic aromatic hydrocarbons in mosses is reported using ultrasonic-assisted extraction and gas chromatography-tandem mass spectrometry. The efficiency of ultrasonic-assisted extraction and the reagents was optimized. Tandem mass spectrometry with selective reaction monitoring was used to enhance the selectivity to reduce matrix interferences and simplify the purification protocol. The detection limits were from 0.1 to 2.0ng/mL. The linear calibration range was two orders of magnitude and the coefficients of linear correlation exceeded 0.9992 for all analytes. The relative standard deviations within 1 day and 3 days were less than 9.0%. Recoveries from 56.8 to 109.0% were obtained in fortified mosses. The rapid, low solvent gas chromatography-tandem mass spectrometry method was used to determine polycyclic aromatic hydrocarbons in mosses.
引用
收藏
页码：243 / 257
页数：15
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