Phase-transfer-catalyzed synthesis of N-aryl-N'-(2-chlorobenzoyl)-thiourea derivatives

被引：16
|
作者：
Zhang, YM
Wei, TB
Wang, LL
机构：
[1] Department of Chemistry, Northwest Normal University, Lanzhou, Gansu
[2] Lanzhou Inst. of Chemical Physics, Chinese Academy of Sciences, Lanzhou, Gansu
来源：
SYNTHETIC COMMUNICATIONS | 1997年 / 27卷 / 05期
关键词：
D O I：
10.1080/00397919708004195
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Reaction of aromatic amines with 8-chlorobenzoyl chloride and ammonium thiocyanate under the condition of solid-liquid phase-transfer catalysis using polyethylene glycol-400 (PEG-400) as the catalyst yielded N-aryl-N'-(2-chlorobenzoyl)thioureas 3a-3j in good to excellent yield.
引用
收藏
页码：751 / 756
页数：6
相关论文
共 50 条
  • [1] Phase transfer catalyzed synthesis of N-aryl-N'-(2-furoyl)thiourea derivatives
    Zhang, YM
    Wei, TB
    [J]. INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 1996, 35 (10): : 1088 - 1090
  • [2] HYDROGEN-BONDS IN DERIVATIVES OF N-SUBSTITUTED N'-BENZOYL-(2-CHLOROBENZOYL)THIOUREA AND N'-(2-CHLOROBENZOYL)THIOUREA
    HRITZOVA, O
    KOSCIK, D
    [J]. COLLECTION OF CZECHOSLOVAK CHEMICAL COMMUNICATIONS, 1991, 56 (04) : 880 - 885
  • [3] Synthesis of N-aryl-N′-undecanoyl thiourea derivatives
    Loloiu, G
    Loloiu, T
    Badicu, N
    Gavriliu, D
    Maior, O
    [J]. REVUE ROUMAINE DE CHIMIE, 2001, 46 (08) : 899 - 903
  • [4] Synthesis, characterization and antimicrobial activities of transition metal complexes of N,N-dialkyl-N′-(2-chlorobenzoyl)thiourea derivatives
    Binzet, Gun
    Arslan, Hakan
    Floerke, Ulrich
    Kuelcue, Nevzat
    Duran, Nizami
    [J]. JOURNAL OF COORDINATION CHEMISTRY, 2006, 59 (12) : 1395 - 1406
  • [5] N-(2-Chlorobenzoyl)-N′(4-nitrophenyl)thiourea
    Yusof, M. Sukeri M.
    Edris, Mustaqim M.
    Mardi, A. Sahali
    Yamin, Bohari M.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O94 - O95
  • [6] N-(2-Chlorobenzoyl)-N′-(3-pyridyl)thiourea
    Chai, Lan-Qin
    Ding, Yu-Jie
    Yang, Xiao-Qing
    Yan, Hai-Bo
    Dong, Wen-Kui
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1407 - U1503
  • [7] Tmeda-catalyzed synthesis of N-aryl-N′-ethoxycarbonyl thiourea and arene (or polymethylene)bis-ethoxycarbonylthiourea derivatives
    Lin, Q
    Zhang, YM
    Gao, LM
    Wei, TB
    Wang, H
    [J]. PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2004, 179 (10) : 2051 - 2057
  • [8] N′-(2-chlorobenzoyl)-n-(pyrrolidin-1-yl)thiourea
    Emen, FM
    Flörke, U
    Külcü, N
    Arslan, H
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 : O1159 - O1160
  • [9] Synthesis of N-aryl-N'-heteroaryl-substituted urea and thiourea derivatives and evaluation of their anticonvulsant activity
    Heinisch, G
    Matuszczak, B
    Rakowitz, D
    Tantisira, B
    [J]. ARCHIV DER PHARMAZIE, 1997, 330 (07) : 207 - 210
  • [10] N-(2-Chlorobenzoyl)benzenesulfonamide
    Gowda, B. Thimme
    Foro, Sabine
    Suchetan, P. A.
    Fuess, Hartmut
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O326 - U2130
12345