Mechanical Alloying of Metal-Organic Frameworks

被引：59

作者：

Panda, Tamas ^{[1
]}

Horike, Satoshi ^{[2
]}

Hagi, Keisuke ^{[2
]}

Ogiwara, Naoki ^{[2
]}

Kadota, Kentaro ^{[2
]}

Itakura, Tomoya ^{[3
]}

Tsujimoto, Masahiko ^{[1
]}

Kitagawa, Susumu ^{[1
,2
]}

机构：

[1] Kyoto Univ, Inst Integrated Cell Mat Sci iCeMS, Sakyo Ku, Yoshida, Kyoto 6068501, Japan

[2] Kyoto Univ, Dept Synthet Chem & Biol Chem, Grad Sch Engn, Nishikyo Ku, Katsura, Kyoto 6158510, Japan

[3] Denso Corp, 1-1 Showa Cho, Kariya, Aichi 4488661, Japan

来源：

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION | 2017年 / 56卷 / 09期

基金：

日本科学技术振兴机构; 日本学术振兴会;

关键词：

alloys; amorphous phases; ball milling; metal-organic frameworks; solid solutions; ZEOLITIC IMIDAZOLATE FRAMEWORKS; POROUS COORDINATION POLYMERS; SOLID-SOLUTIONS; STABILITY;

D O I：

10.1002/anie.201612587

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The solvent-free mechanical milling process for two distinct metal-organic framework (MOF) crystals induced the formation of a solid solution, which is not feasible by conventional solution-based syntheses. X-ray and STEM-EDX studies revealed that performing mechanical milling under an Ar atmosphere promotes the high diffusivity of each metal ion in an amorphous solid matrix; the amorphous state turns into the porous crystalline structure by vapor exposure treatment to form a new phase of a MOF solid solution.

引用

页码：2413 / 2417

页数：5

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