Synthesis and structural characterization of calcium hypophosphite

被引:0
|
作者
Ai Qingxue [1 ]
Wang Fusheng [1 ]
Guo Aihong [2 ]
机构
[1] North China Univ Sci & Technol, Sch Min Engn, Tangshan, Hebei, Peoples R China
[2] North China Univ Sci & Technol, Sch Chem Engn, Tangshan, Hebei, Peoples R China
来源
PROCEEDINGS OF THE 2016 INTERNATIONAL FORUM ON ENERGY, ENVIRONMENT AND SUSTAINABLE DEVELOPMENT (IFEESD) | 2016年 / 75卷
关键词
calcium hypophosphite; synthesis; characterization;
D O I
暂无
中图分类号
X [环境科学、安全科学];
学科分类号
08 ; 0830 ;
摘要
Calcium hypophosphate is got from sodium hypophosphite and sodium chloride. The internal morphology and composition of calcium hypophosphate particles are obtained by nanometer particle sizer, scanning electron microscope (SEM) and X-ray diffraction (XRD) and also on. The experimental results show that 2.0 mol/L, 40 degrees C, 100 min under the conditions can get large yield and particle size is minimal about 0.563 mu m. Calcium hypophosphate is high purity, structure likes rod, and the content of Phosphorus element is high. The method is feasible and subsequent treatment is simple.
引用
收藏
页码:1048 / 1052
页数:5
相关论文
共 50 条
  • [1] Non-Halogen Flame Retardant Synthesis and Structural Characterization of Calcium Hypophosphite
    Ai, Qingxue
    Wang, Fusheng
    Guo, Aihong
    2016 INTERNATIONAL CONFERENCE ON MECHANICAL MANUFACTURING AND ENERGY ENGINEERING (ICMMEE 2016), 2016, : 190 - 196
  • [2] Synthesis and structural characterization of substituted calcium hexaferrites
    Umashankararaja, R.
    Manjunatha, B. C.
    Rajashekara, K. M.
    MATERIALS TODAY-PROCEEDINGS, 2021, 37 : 742 - 744
  • [3] In vitro synthesis and structural characterization of amorphous calcium carbonate
    Günther, C
    Becker, A
    Wolf, G
    Epple, M
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2005, 631 (13-14): : 2830 - 2835
  • [4] Synthesis and structural characterization of microporous yttrium and calcium silicates
    Rocha, J
    Ferreira, P
    Lin, Z
    Brandao, P
    Ferreira, A
    de Jesus, JDP
    JOURNAL OF PHYSICAL CHEMISTRY B, 1998, 102 (24): : 4739 - 4744
  • [5] Synthesis and characterization of a polycarboxylate superplasticizer modified by sodium hypophosphite
    Zhang, Ming
    Wang, Luyan
    Zhang, Xiuzhi
    Mi, Xiangyun
    Sun, Fengmeng
    Ding, Mei
    Pei, Meishan
    POLYMERS FOR ADVANCED TECHNOLOGIES, 2022, 33 (05) : 1442 - 1456
  • [6] SYNTHESIS AND CHARACTERIZATION OF BINUCLEAR OXO MOLYBDENUM(V) HYPOPHOSPHITE
    SASTRY, MS
    KULSHRESHTHA, SK
    TRANSITION METAL CHEMISTRY, 1989, 14 (04) : 248 - 250
  • [7] Synthesis and characterization of bimetal phosphide NiCoP by reduction of hypophosphite
    Tong, Jian-Bo
    Liu, Ying-Ying
    Liu, Shu-Ling
    Rengong Jingti Xuebao/Journal of Synthetic Crystals, 2015, 44 (01): : 155 - 160
  • [8] Synthesis and structural characterization of calcium titanate by spray pyrolysis method
    Lanfredi, S.
    Storti, F.
    Simoes, L. P. M.
    Djurado, E.
    Nobre, M. A. L.
    MATERIALS LETTERS, 2017, 201 : 148 - 151
  • [9] SYNTHESIS AND STRUCTURAL CHARACTERIZATION OF LAYERED CALCIUM AND LANTHANIDE PHOSPHONATE SALTS
    CAO, G
    LYNCH, VM
    SWINNEA, JS
    MALLOUK, TE
    INORGANIC CHEMISTRY, 1990, 29 (11) : 2112 - 2117
  • [10] New bismuth calcium oxysilicate with apatite structure: Synthesis and structural characterization
    Uvarov, Vladimir
    Shenawi-Khalil, Sanaa
    Popov, Inna
    JOURNAL OF SOLID STATE CHEMISTRY, 2010, 183 (07) : 1484 - 1489