(E)-2-(Isonicotinoylhydrazonomethyl)benzoic acid methanol monosolvate

被引:0
|
作者
Li, Wenkuan
Yin, Handong
Wen, Liyuan
Cui, Jichun
Wang, Daqi
机构
[1] College of Chemistry and Chemical Engineering, Liaocheng University
关键词
D O I
10.1107/S1600536809038902
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C14H11N3O3 center dot CH4O, was synthesized by the condensation reaction of isonicotinohydrazide with an equimolar quantity of 2-formylbenzoic acid in methanol. The hydrazone molecule displays an E configuration about the C=N bond. The dihedral angel between the pyridine and the benzene rings is 12.04 (5)degrees. In the crystal structure, molecules are linked by O-H center dot center dot center dot N, O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen-bonding interactions.
引用
收藏
页码:O2578 / +
页数:8
相关论文
共 50 条
  • [1] 2-(4-Dimethylamino-2-hydroxybenzoyl)benzoic acid methanol solvate
    Guo, Jin-Chun
    Liu, Qing-Hao
    Guo, Jin-Ying
    Chen, Mei-Zhu
    Zhang, Rui-Wang
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O2419 - U3118
  • [2] Eucomic acid methanol monosolvate
    Li, Guo-Qiang
    Li, Yao-Lan
    Wang, Guo-Cai
    Liang, Zhi-Hong
    Jiang, Ren-Wang
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2192 - U1940
  • [3] 4-{(E)-N′-[2-(8-Quinolyloxy)acetyl]hydrazonomethyl}benzoic acid methanol solvate
    Ren, Chun-Yan
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : 01601 - U2674
  • [4] 2-[(E)-(1,10-Phenanthrolin-5-yl) iminomethyl] phenol methanol monosolvate
    Yildirim, Sema Oeztuerk
    Demirhan, Nebahat
    Elmali, Fikriye
    Butcher, Ray J.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1173 - U2773
  • [5] 2-(isopropylthio)benzoic acid
    Gerkin, RE
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1999, 55 : 1190 - 1192
  • [6] 2-(Trifluoromethyl)benzoic acid
    Betz, Richard
    Gerber, Thomas
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O907 - U822
  • [7] 2-(Dibromomethyl)benzoic acid
    Lin, Hong-Yi
    Fang, Sin-Kai
    Chen, Kew-Yu
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68
  • [8] 2-[2-(hydroxyethyl)phenoxy]benzoic acid
    Damas, AM
    Roleira, FF
    Pinto, MMM
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1997, 53 : 1143 - 1145
  • [9] 2-(2-Carboxyethyl)-1,3-dioxoisoindoline-5,6-dicarboxylic acid methanol monosolvate
    Khorasani, Sanaz
    Fernandes, Manuel A.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68
  • [10] 2-(Morpholinium-4-yl)ethylammonium sulfate methanol monosolvate
    Bi, Ye
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O951 - U3309