Synthesis, crystal structure, and spectral characteristics of N-(tert-butyl)aminomethanesulfonic acid

被引:5
|
作者
Khoma, R. E. [1 ,2 ]
Gel'mbol'dt, V. O. [3 ]
Ennan, A. A. [1 ]
Baumer, V. N. [4 ,5 ]
Puzan, A. N. [4 ]
机构
[1] Natl Acad Sci Ukraine, Minist Educ & Sci, Physicochem Inst Human & Environm Protect, UA-65082 Odessa, Ukraine
[2] Mechnikov Odessa Natl Univ, Odessa, Ukraine
[3] Odessa Natl Med Univ, Odessa, Ukraine
[4] Natl Acad Sci Ukraine, Inst Single Crystals, Kharkov, Ukraine
[5] Kharkov Natl Univ, Kharkov, Ukraine
关键词
sulfur(IV) oxide; paraformaldehyde; primary alkylamine; condensation; BUFFERS;
D O I
10.1134/S1070363215100102
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A new method of the synthesis of N-(tert-butyl)aminomethanesulfonic acid in the system SO2-(CH3)(3)CNH2-CH2O-H2O was developed. The target compound [(CH3)(3)D]NHCH2SO3H was characterized by means of X-ray diffraction analysis, IR spectroscopy, and mass spectrometry.
引用
收藏
页码:2282 / 2284
页数:3
相关论文
共 50 条
  • [1] Synthesis, crystal structure, and spectral characteristics of N-(tert-butyl)aminomethanesulfonic acid
    R. E. Khoma
    V. O. Gel’mbol’dt
    A. A. Ennan
    V. N. Baumer
    A. N. Puzan
    [J]. Russian Journal of General Chemistry, 2015, 85 : 2282 - 2284
  • [2] Synthesis, Crystal Structure, and Spectral Characteristics of N-(Hydroxyethyl)aminomethanesulfonic Acid
    Khoma, R. E.
    Gel'mbol'dt, V. O.
    Shishkin, O. V.
    Baumer, V. N.
    Koroeva, L. V.
    [J]. RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2013, 83 (05) : 969 - 971
  • [3] Synthesis, crystal structure, and spectral characteristics of N-(Hydroxyethyl)aminomethanesulfonic acid
    R. E. Khoma
    V. O. Gel’mbol’dt
    O. V. Shishkin
    V. N. Baumer
    L. V. Koroeva
    [J]. Russian Journal of General Chemistry, 2013, 83 : 969 - 971
  • [4] Synthesis and Crystal Structure of 4-(tert-butyl)-N-(pyridin-3-ylmethyl) benzenesulfonamide
    Balu, K.
    Gopalan, R. Srinivasa
    [J]. JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2013, 43 (08) : 409 - 411
  • [5] Synthesis and Crystal Structure of 4-(tert-butyl)-N-(pyridin-3-ylmethyl) benzenesulfonamide
    K. Balu
    R. Srinivasa Gopalan
    [J]. Journal of Chemical Crystallography, 2013, 43 : 409 - 411
  • [6] tert-butyl N-(phosphinoyloxy) carbamate
    Blatch, Alexandrea J.
    Howard, Judith A. K.
    Probert, Michael R.
    Smethurst, Christian A.
    Whiting, Andrew
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O5346 - O5348
  • [7] Synthesis, crystal structure and Hirshfeld surface analysis of tert-butyl N-acetylcarbamate
    El Mestehdi, Aly Dawa
    Abba, Moctar
    El Housseine, Mohamed Lemine
    Hadou, Abderrahmane Ould
    Barry, Aliou Hamady
    Elemine, Brahim Ould
    Jelsch, Christian
    Gaye, Mohamed
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2022, 78 : 1072 - +
  • [8] Synthesis and crystal structure of hexa(tert-butyl)bismocenium tetrachloroaluminate
    Sitzmann, H
    Wolmershauser, G
    [J]. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 1997, 52 (03): : 398 - 400
  • [9] A CONVENIENT SYNTHESIS OF TERT-BUTYL N-(2-BROMOETHYL)CARBAMATE
    BEYLIN, VG
    GOEL, OP
    [J]. ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 1987, 19 (01) : 78 - 80
  • [10] Synthesis, crystal structure and spectroscopic properties of a novel carbacylamidophosphate: N-(3-nitrobenzoyl)-N′,N"-bis(tert-butyl)phosphoric triamide
    Gholivand, Khodayar
    Mostaanzadeh, Hossein
    Koval, Tomas
    Dusek, Michal
    Erben, Mauricio F.
    Della Vedova, Carlos O.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 2009, 65 : 502 - 508