Determination of alkaloids in Sinomenium acutum by field-amplified sample stacking in capillary electrophoresis with chemiluminescene detection

被引：10
|
作者：
Shi, Guiying
Li, Jiang
Yin, Yingchun
Xu, Xueqin [1 ]
Chen, Guonan
机构：
[1] Fuzhou Univ, Dept Chem, Fuzhou 350108, Fujian, Peoples R China
来源：
LUMINESCENCE | 2013年 / 28卷 / 04期
关键词：
capillary electrophoresis; chemiluminescene; field-amplified sample stacking; Sinomenium acutum; alkaloids;
D O I：
10.1002/bio.2478
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
ABS A simple and rapid capillary electrophoresis (CE) with an acidic potassium permanganate chemiluminescence (CL) detection method was developed to determine three alkaloids (curine, sinomenine and magnoflorine) simultaneously. A laboratory-built CE-CL detection interface was used. Sinomenium acutum, and the result of the determination of sinomenine was in good agreement with those given by high-performance liquid chromatography and CE methods. In addition, a possible CL reaction mechanism of sinomenine-KMnO4-H2SO4 was proposed. Copyright (c) 2013 John Wiley & Sons, Ltd.
引用
收藏
页码：468 / 473
页数：6
相关论文
共 50 条
  • [1] Field-amplified sample stacking in capillary electrophoresis for the determination of alkaloids in Sinomenium acutum
    Wang, Lili
    Xu, Huifeng
    Ye, Hongzhi
    Yu, Lishuang
    Lin, Zhenyu
    Liu, Xianxiang
    Chen, Guonan
    ANALYTICAL METHODS, 2013, 5 (19) : 5267 - 5271
  • [2] Determination of monoamines in urine by capillary electrophoresis with field-amplified sample stacking and amperometric detection
    Weng, QF
    Xu, GW
    Yuan, KL
    Tang, P
    JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES, 2006, 835 (1-2): : 55 - 61
  • [3] Determination of amphetamines in hair by capillary zone electrophoresis with field-amplified sample stacking
    Meng Pinjia
    CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2006, 34 (08) : 1137 - 1140
  • [4] Capillary electrophoresis determination of biogenic amines by field-amplified sample stacking and in-capillary derivatization
    García-Villar, N
    Saurina, J
    Hernández-Cassou, S
    ELECTROPHORESIS, 2006, 27 (02) : 474 - 483
  • [5] Capillary electrophoresis with field-amplified sample stacking for rapid and sensitive determination of sulfadiazine and sulfamethoxazole
    Li, Yuqin
    Cui, Yingjie
    Jia, Baoxiu
    Wang, Hao
    Liu, Caihong
    Qi, Yongxiu
    PHARMAZIE, 2012, 67 (09): : 768 - 773
  • [6] Determination of metformin in plasma by capillary electrophoresis using field-amplified sample stacking technique
    Song, JZ
    Chen, HF
    Tian, SJ
    Sun, ZP
    JOURNAL OF CHROMATOGRAPHY B, 1998, 708 (1-2): : 277 - 283
  • [7] Field-amplified sample stacking-sweeping of vitamins B determination in capillary electrophoresis
    Dziomba, Szymon
    Kowalski, Piotr
    Baczek, Tomasz
    JOURNAL OF CHROMATOGRAPHY A, 2012, 1267 : 224 - 230
  • [8] Subcritical water extraction of alkaloids in Sophora flavescens Ait. and determination by capillary electrophoresis with field-amplified sample stacking
    Wang, Haiyan
    Lu, Yuchao
    Chen, Jie
    Li, Junchao
    Liu, Shuhui
    JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2012, 58 : 146 - 151
  • [9] Determination of sinomenine in Sinomenium acutum by capillary electrophoresis with electrochemiluminescence detection
    Zhou, Min
    Ma, Yong-Jun
    Ren, Xiao-Na
    Zhou, Xiu-Ying
    Li, Li
    Chen, Hui
    ANALYTICA CHIMICA ACTA, 2007, 587 (01) : 104 - 109
  • [10] Rapid and sensitive determination of posaconazole in patient plasma by capillary electrophoresis with field-amplified sample stacking
    Liao, Hsiao-Wei
    Lin, Shu-Wen
    Wu, Un-In
    Kuo, Ching-Hua
    JOURNAL OF CHROMATOGRAPHY A, 2012, 1226 : 48 - 54
12345