A Novel Research on Behavior of Zinc Ferrite Nanoparticles in Different Concentration of Poly(vinyl pyrrolidone) (PVP)

被引:24
|
作者
Kamari, Halimah Mohamed [1 ,2 ]
Naseri, Mahmoud Goodarz [3 ]
Saion, Elias B. [1 ,2 ]
机构
[1] Univ Putra Malaysia, Dept Phys, Upm Serdang 43300, Selangor, Malaysia
[2] Univ Putra Malaysia, Dept Phys, Upm Serdang 43400, Selangor, Malaysia
[3] Malayer Univ, Fac Sci, Dept Phys, Malayer 6571995863, Iran
来源
METALS | 2014年 / 4卷 / 02期
关键词
nanocrystals; magnetic properties; poly(vinyl pyrrolidone); thermal treatment; MAGNETIC-PROPERTIES; NICKEL FERRITE; NANOCRYSTALS; EVOLUTION; COPOLYMER; NIFE2O4;
D O I
10.3390/met4020118
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Zinc ferrite nanocrystals were prepared from an aqueous solution containing metal nitrates and various of concentrations of poly(vinyl pyrrolidone) (PVP), i.e., 0, 15, 40, and 55 g/L, as a capping agent. To stabilize the particles, they were thermally treated at 873 K, as an optimum calcination temperature. The behaviors of the polymeric precursor were analyzed by use of simultaneous thermo-gravimetry (TG) and derivative thermo-gravimetry analyses (DTG). The presence of the crystalline phase in each sample was confirmed by X-ray diffraction (XRD) analysis. The average particle size and the morphology of the nanoparticles were determined by transmission electron microscopy (TEM), and these parameters were found to differ at various concentrations of PVP. Fourier transform infrared spectroscopy (FT-IR) confirmed the presence of metal oxide bands for all the PVP concentrations and confirmed the absence of organic bands for PVP concentrations less than 55 g/L. Measurements of the magnetization value of the zinc ferrite nanoparticles were obtained at room temperature by using a vibrating sample magnetometer (VSM), which showed that, in the absence of PVP, the sample exhibited a paramagnetic behavior while, in the presence of PVP, samples have a super-paramagnetic behavior.
引用
收藏
页码:118 / 129
页数:12
相关论文
共 50 条
  • [1] Preparing AgBr nanoparticles in poly(vinyl pyrrolidone) (PVP) nanofibers
    Bai, Jie
    Li, Yaoxian
    Zhang, Chaoqun
    Liang, Xiaofei
    Yang, Qingbiao
    [J]. COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS, 2008, 329 (03) : 165 - 168
  • [2] Synthesis and characterization of poly (vinyl pyrrolidone) (PVP)
    Yang, B
    Zhang, YQ
    Tian, L
    [J]. PROGRESS OF FINE CHEMISTRY AND FUNCTIONAL POLYMERS, 1998, : 244 - 246
  • [3] Characterization of Zinc Ferrite Nanoparticles Capped with Different PVP Concentrations
    Z. Alsayed
    M. S. Badawi
    R. Awad
    [J]. Journal of Electronic Materials, 2019, 48 : 4925 - 4933
  • [4] Characterization of Zinc Ferrite Nanoparticles Capped with Different PVP Concentrations
    Alsayed, Z.
    Badawi, M. S.
    Awad, R.
    [J]. JOURNAL OF ELECTRONIC MATERIALS, 2019, 48 (08) : 4925 - 4933
  • [5] Synthesis and Characterization of High-Transparent Poly(vinyl alcohol)/Poly(vinyl pyrrolidone)(PVA/PVP) Hydrogels
    XU Yi
    ZHOU Gang
    LIU Lei
    LIU Hong-ru
    LIU Hai-feng
    NIU Xu-feng
    FAN Yu-bo
    [J]. Chinese Journal of Biomedical Engineering, 2018, 27 (01) : 23 - 27
  • [6] MISCIBILITY AND ORIENTATION BEHAVIOR OF POLY(VINYL ALCOHOL) POLY(VINYL PYRROLIDONE) BLENDS
    NISHIO, Y
    HARATANI, T
    TAKAHASHI, T
    [J]. JOURNAL OF POLYMER SCIENCE PART B-POLYMER PHYSICS, 1990, 28 (03) : 355 - 376
  • [7] Effect of citrate on poly(vinyl pyrrolidone)-stabilized gold nanoparticles formed by PVP reduction in microwave (MW) synthesis
    Seol, Seung Kwon
    Kim, Daeho
    Jung, Sunshin
    Chang, Won Suk
    Bae, Young Min
    Lee, Kyeong Hee
    Hwu, Yeukuang
    [J]. MATERIALS CHEMISTRY AND PHYSICS, 2012, 137 (01) : 135 - 139
  • [8] Synthesis of poly(vinyl pyrrolidone)-stabilied silver nanoparticles
    Yiamsawas, Doungporn
    Lauruengtana, Vichuta
    Ruktanonchai, Uracha
    Kangwansupamongkon, Wiyong
    [J]. 2007 2ND IEEE INTERNATIONAL CONFERENCE ON NANO/MICRO ENGINEERED AND MOLECULAR SYSTEMS, VOLS 1-3, 2007, : 860 - +
  • [9] Morphology, drug release behavior, thermal, and mechanical properties of poly(ethylene oxide) (PEO)/poly(vinyl pyrrolidone) (PVP) blends
    Sedeh, Negar Naghdi
    Entezam, Mehdi
    Jafari, Seyed Hassan
    Khonakdar, Hossein-Ali
    Abdouss, Majid
    [J]. JOURNAL OF APPLIED POLYMER SCIENCE, 2018, 135 (26)
  • [10] Thermal behavior of poly(acrylic acid)-poly(vinyl pyrrolidone) and poly(acrylic acid)-metal-poly(vinyl pyrrolidone) complexes
    Moharram, M. A.
    Khafagi, M. G.
    [J]. JOURNAL OF APPLIED POLYMER SCIENCE, 2006, 102 (04) : 4049 - 4057