trans-Diaquabis(N,N-dimethylethane-1,2-diamine-κ2N,N′)nickel(II) dichloride dihydrate:: a redetermination at 90 K

被引：5

作者：

Ide, Daniela M. M. ^{[1
]}

Norman, Richard E. ^{[1
]}

机构：

[1] Sam Houston State Univ, Dept Chem, Huntsville, TX 77341 USA

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2007年 / 63卷

关键词：

D O I：

10.1107/S1600536807002140

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The crystal structure of the centrosymmetric title compound, [Ni(C4H12N2)(2)(H2O)(2)]Cl-2 center dot 2H(2)O, has been reported previously at room temperature by Ihara, Satake, Fujimoto, Senda, Suzuki & Uehara [Bull. Chem. Soc. Jpn (1991), 64, 2349 - 2352]. At room temperature, the five-membered chelate ring displays disorder over gauche and eclipsed conformations, whereas at 90 K no such disorder is observed. The present redetermination shows better agreement of bond lengths with expected values.

引用

页码：M558 / M560

页数：3

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