Kinetics of the pre-treatment of used cooking oil using Novozyme 435 for biodiesel production

被引：5

作者：

Haigh, K. F. ^{[1
]}

Saha, B. ^{[2
]}

Vladisavljevic, G. T. ^{[1
]}

Reynolds, J. C. ^{[3
]}

机构：

[1] Univ Loughborough, Dept Chem Engn, Loughborough LE11 4LE, Leics, England

[2] London South Bank Univ, Fac Engn Sci & Built Environm, Dept Appl Sci, London SE1 0AA, England

[3] Univ Loughborough, Dept Chem, Loughborough LE11 4LE, Leics, England

来源：

CHISA 2012 | 2012年 / 42卷

基金：

英国工程与自然科学研究理事会;

关键词：

Biodiesel; liquid chromatography; Novozyme; 435; esterfication; transeterifcation; PERFORMANCE LIQUID-CHROMATOGRAPHY; TRANSESTERIFICATION; MECHANISMS; LIPASE;

D O I：

10.1016/j.proeng.2012.07.502

中图分类号：

TQ [化学工业];

学科分类号：

0817 ;

摘要：

The pretreatment of used cooking oil (UCO) for the preparation of biodiesel has been investigated, using Novozyme 435, Candida antarctica Lipase B immobilized on acrylic resin, as the catalyst. The reactions in UCO were carried out using a jacketed batch reactor with a reflux condenser. The liquid chromatography mass spectrometry (LC-MS) method was developed to monitor the mono-, di and triglyceride concentrations for this work and it has been shown that it is possible to obtain linear calibration curves. This work showed that Novozyme 435 will catalyse the esterification of FFAs and the transesterification of mono- and diglycerides typically found in UCO when Novozyme 435 is used to catalyse the pretreatement of UCO for the formation of biodiesel. (C) 2012 Published by Elsevier Ltd.

引用

页码：1106 / 1113

页数：8

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