Extraction of cellulose from pistachio shell and physical and mechanical characterisation of cellulose-based nanocomposites

被引:29
|
作者
Movva, Mounika [1 ]
Kommineni, Ravindra [2 ]
机构
[1] PVP Siddhartha Inst Technol, Mech Engn Dept, Vijayawada, Andhra Prades, India
[2] RVR & JC Coll Engn, Mech Engn Dept, Guntur, Andhra Prades, India
来源
MATERIALS RESEARCH EXPRESS | 2017年 / 4卷 / 04期
关键词
nanocellulose; pistachio; tensile strength; flexural strength; polymer composites; FIBER; NANOCRYSTALS; PYROLYSIS;
D O I
10.1088/2053-1591/aa6863
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Cellulose is an important nanoentity that have been used for the preparation of composites. The present work focuses on the extraction of cellulose from pistachio shell and preparing a partially degradable nanocomposite with extracted cellulose. Physical and microstructural characteristics of nanocellulose extracted from pistachio shell powder (PSP) through various stages of chemical treatment are identified from scanning electron microscopy (SEM), Fourier transform infra-red spectroscopy (FTIR), x-ray powder diffraction (XRD), and thermogravimetric analysis (TGA). Later, characterized nanocellulose is reinforced in a polyester matrix to fabricate nanocellulose-based composites according to the ASTM standard. The resulting nanocellulose composite performance is evaluated in the mechanical perspective through tensile and flexural loading. SEM, FTIR, and XRD showed that the process for extraction is efficient in obtaining 95% crystalline cellulose. Cellulose also showed good thermal stability with a peak thermal degradation temperature of 361 degrees C. Such cellulose when reinforced in a matrix material showed a noteworthy rise in tensile and flexural strengths of 43 MPa and 127 MPa, at a definite weight percent of 5%.
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页数:9
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