Crystallization Process and Magnetic Properties of Amorphous NiFe2O4 Nanoparticles

被引:2
|
作者
Nguyen Dang Phu [1 ]
Nguyen Van Hung [1 ]
Luc Huy Hoang [1 ]
Nguyen Van Minh [1 ]
Le Mai Oanh [1 ]
Danh Bich Do [1 ]
机构
[1] Hanoi Natl Univ Educ, Fac Phys, Hanoi 10000, Vietnam
关键词
Amorphous materials; ferrite; magnetic particles; magnetic properties; MICROWAVE-ASSISTED PREPARATION; IRON-OXIDE; SONOCHEMICAL SYNTHESIS; ELECTRODES; SPECTRA; FE;
D O I
10.1109/TMAG.2013.2297520
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
We investigate the crystallization process of NiFe2O4 nanoparticles prepared by microwave heating technique, which were then characterized using X-ray diffraction, high-resolution transmission electron microscopy, the differential scanning calorimetry, Raman scattering, Fourier transformed infrared spectra (FTIR), and magnetic measurements. The results showed that crystallization of the amorphous NiFe2O4 nanoparticles occurred at around 300 degrees C. The best crystallization quality would be obtained by annealing the sample at 500 degrees C. After crystallization, the sample shows ferromagnetic behavior with a saturation magnetization of about 30 emu/g. The FTIR and Raman measurements also provided further information about the crystallization process and the phase transformation of the NiFe2O4 nanoparticles.
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页数:4
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