Three Dimensional Reconstruction of Solid Oxide Fuel Cell Electrodes Using Focused Ion Beam - Scanning Electron Microscopy

被引：24

作者：

Wilson, James R. ^{[1
]}

Kobsiriphat, Worawarit ^{[1
]}

Mendoza, Roberto ^{[1
,3
]}

Chen, Hsun-Yi ^{[3
]}

Hines, Tom ^{[1
]}

Hiller, Jon M. ^{[2
]}

Miller, Dean J. ^{[2
]}

Thornton, Katsuyo ^{[3
]}

Voorhees, Peter W. ^{[1
]}

Adler, Stuart B. ^{[4
]}

Mumm, Daniel ^{[5
]}

Barnett, Scott A. ^{[1
]}

机构：

[1] Northwestern Univ, Dept Mat Sci, Evanston, IL 60208 USA

[2] Argonne Natl Lab, Argonne, IL 60439 USA

[3] Univ Michigan, Dept Mat Sci, Ann Arbor, MI 48109 USA

[4] Univ Washington, Dept Chem Engn, Seattle, WA 98195 USA

[5] Univ Calif Irvine, Dept Chem Engn & Mat Sci, Irvine, CA 92697 USA

来源：

SOLID OXIDE FUEL CELLS 10 (SOFC-X), PTS 1 AND 2 | 2007年 / 7卷 / 01期

基金：

美国国家科学基金会;

关键词：

D O I：

10.1149/1.2729300

中图分类号：

O646 [电化学、电解、磁化学];

学科分类号：

081704 ;

摘要：

Solid oxide fuel cell (SOFC) electrodes typically consist of contiguous electronically and ionically conducting solid phases in an interconnected porous structure. Quantitatively analyzing this microstructure remains a key challenge in connecting materials processing with electrode performance. This paper will describe the application of dual-beam focused ion beam - scanning electron microscopy for three-dimensional reconstruction of Ni-YSZ cermet anodes, LSM-YSZ cathodes, and (La,Sr)CoO3 cathodes. Different methods for segmentation, i.e. converting images to 3D data sets, are compared and the tradeoff between calculation accuracy and analysis time is discussed.

引用

页码：1879 / +

页数：2

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