Hydrothermal synthesis of Ni-Fe layered double hydroxide with high crystallinity using homogeneous precipitation method

被引：4
|
作者：
Zhang, Yingchao [1 ]
机构：
[1] Beijing Solar Energy Res Inst Co Ltd, Beijing 100012, Peoples R China
来源：
ADVANCES IN TEXTILE ENGINEERING AND MATERIALS III, PTS 1 AND 2 | 2013年 / 821-822卷
关键词：
Layered double hydroxide; Hydrothermal synthesis; Homogeneous precipitation;
D O I：
10.4028/www.scientific.net/AMR.821-822.1313
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Ni-Fe layered double hydroxide containing carbonate anion (CO32-) has been successfully synthesized by a process of homogeneous precipitation involving urea hydrolysis under hydrothermal conditions. Factors that influence the composition and the crystallinity degree of NiFe-LDH, such as the molar fraction of urea/NO3- in solution, the total metal ion concentration in solution and the aging time, have been investigated in detail. Structure and morphology of the sample were characterized by X-ray powder diffraction (XRD), Fourier transform infrared (FT-IR) spectra and scanning electron microscope (SEM). The results indicate NiFe-LDH with high purity present well-crystalline, uniform crystallite size
引用
收藏
页码：1313 / 1316
页数：4
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