Investigation of stacking disorder in Li2SnO3

被引:19
|
作者
Tarakina, N. V. [1 ]
Denisova, T. A. [1 ]
Maksimova, L. G. [1 ]
Baklanova, Y. V. [1 ]
Tyutyunnik, A. P. [1 ]
Berger, I. F. [1 ]
Zubkov, V. G. [1 ]
van Tendeloo, G. [2 ]
机构
[1] Russian Acad Sci, Inst Solid State Chem, Ural Branch, Ekaterinburg 620041, Russia
[2] Univ Antwerp, EMAT, B-2020 Antwerp, Belgium
关键词
diffuse scattering; stacking disorder; microstructure; powder diffraction; electron diffraction; LITHIUM CERAMICS; TEMPERATURE;
D O I
10.1524/zksu.2009.0055
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
A crystal structure investigation of the low temperature Li2SnO3 modification has been carried out. X-ray, neutron powder and electron diffraction data showed that this compound crystallizes in a monoclinic unit cell with parameters: a = 5.3033(2)angstrom, b = 9.1738(3)angstrom, c = 10.0195(2)angstrom, beta similar to 100.042(2)degrees and has stacking disorder along the c-axis. Simulation of diffraction patterns with different stacking faults mainly reveal the presence of rotational stacking faults with a probability of about 40%
引用
收藏
页码:375 / 380
页数:6
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